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885 Jarvis DrIve <br /> Sequoia Morgan(07'6- <br /> FA)((4o8)78Z-6308 <br /> Analytical www sequ°ialatn corn <br /> Blaine Tech Services(Shell) Project Shell Sampled 4118/00 <br /> 1680 Rogers Avenue Project Number 2575 Country Club,Stockton Received 4119/00 <br /> San Jose,CA 95112 Project Manager Nick Sudano Reported 5/16/00 11 12 <br /> Volatile Organic Oxygenated Compounds by EPA Method 8260A/Quality Control <br /> Sequoia Analytical-San Carlos <br /> Date Spike Sample QC Reporting Limit Recov RPD RPD <br /> Analyte Anal zed Level Result Result Units Recov Limits % Limit % Notes* <br /> Blank(continued) 0040136-BLKI <br /> h1ethyl tert-butyl ether 4128/00 ND ug/I 200 <br /> Di-isopropyl ether ND 200 <br /> Ethvl tert-butyl ether ND 200 <br /> Tert-amyl methyl ether _ _ ND 200 _ <br /> Surrogate 1,2-Dichloroethane-d4 500 49S 76 0-114 996 <br /> Blank 0040136-BLK2 <br /> Ethanol 4/28/00 ND ug/I 1000 <br /> Tert-butyl alcohol ND 100 <br /> Methyl te-t-butyl ether ND 200 <br /> Di-isopropvr ether ND 200 <br /> Ethyl tert-butyl ether ND 200 <br /> 0cert-amyl methyl ether ND 2_00 <br /> ur,ogate 1 7-Dic doroethane-dot 500 5U6 760-114 101 <br /> LCS 0040136-BSI <br /> _Met_hyl tert-butyl ether _ _4/28/00 500 _ 48 1— ug/l 700-130 962 <br /> Surrogate 1,2-Dichloroethane-d4 1500 492 76 0-114 984 <br /> LCS 0040136-BS2 <br /> Methyl tert-_butyl ether _ __ 4_/28/00 50 0 _ _ 494 ug/I _ _ 700-130 98 8 <br /> 5rtrrogate 1 2-Dichloroethane-d4 50 0 496 760-114 992 <br /> Matrix Suike 0040136-MSI MJD0586-18 <br /> Methyl tert-butyl ether _ 4/2_8/00 _ 500 _ND 507 _ ug/l __60 0-140__ 101_ _ <br /> Surrogate 12-Dtchloroethane-d4 50 D 48 2 76 0-114 96 4 <br /> Matrix Spike Dun 0040136-MSD1 MJD0586-18 <br /> M_ethy_i tert-_butyl ether _ 4/28/00---50 0 _ _ ND_ __51 0 ug/l _ 60 0_-140 102 250 0 985 - <br /> Surrogate 12-Drchloroethane-d4 500 48 9 760-114 978 <br /> 4Vequoia Analytical-Morgan Hill *Refer to end of report for text of nates and definitions <br /> Page 19 of 20 <br />