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S�CltI01a 680 Chesapeake Drive Redwood City CA 94063 (650)364-9600 fAX(650)364-9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (925)988-9600 FAX(925)988-9673 <br /> a- ) <br /> Analytical 819 Striker Avenue Suite 8 Sacramento CA 95834 (916)921-9600 FAX(916)921-0100 <br /> 1455 McDowell Blvd North Ste D Petaluma.CA 94954 (707)792-1865 FAX(707)792-0342 <br /> Blaine Tech Services, Inc Client Project ID Shell 2575 Country Club Blvd <br /> 1680 Rogers Ave Matrix Liquid <br /> San Jose, CA 95112 <br /> Attention Fran Thie Work Order# 9807H87 -06, 08-09, Reported Aug 20, 1998 <br /> 9807H88-10-13 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte Methanol Ethanol iso-Propanol <br /> OC Batch#. GC0731981SHSHSB GC0731981SHSHSB GC0731981SHSHSB <br /> Analy Method- ISHS ISHS ISHS <br /> Prep Method: HS HS HS <br /> Analyst. T Sorokin T Sorokin T Sorokin <br /> MS/MSD# 9807H85o2 98071-18502 9807H8502 <br /> Sample Cone N D N D N D <br /> Prepared Date 7/31/98 7/31/98 7/31/98 <br /> Analyzed Date 7/31/98 7/31/98 7/31/98 <br /> Instrument I D # GCv1 GCv1 Gcv1 <br /> Cone Spiked 8 0 mg/L 8 0 mg/L 8 0 mg/L <br /> Result 87 10 11 <br /> MS % Recovery 109 125 138 <br /> Dap. Result. 90 10 11 <br /> MSD % Recov ' 113 125 138 <br /> RPD 34 00 00 <br /> RPD Limit 0-50 0-50 0-50 <br /> i <br /> I <br /> LCS # BLK073198 BLK073198 ELK073198 <br /> i <br /> Prepared Date 7/31/98 7/31/98 7/31/98 <br /> Analyzed Date- 8/1/98 8/1/98 8/1/98 <br /> Instrument I D # GCV1 GCv1 GCv1 <br /> Cone Spiked- 8 0 mg/L 8 0 mg/L 8 0 mg/L <br /> LCS Result 83 92 98 <br /> LCS % Recov - 104 115 123 <br /> 50-150 50-150 50-150 <br /> LCS 70-130 70-130 70-130 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> A ICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> 40Man <br /> nerager **MS=Matrix Spike, MSD=MS Duplicate, RPD=Relative 9a Difference 9807H87 BLA <1> <br />