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VOC ANALYTICAM ENDALE PAGE 2 QC REPORT FORIW 514 DATE PRINTED 04 DEC 1997 NON-AQUEOUS SAMPLES ------ METHOD BLANK ------ --------------- LAB CONTROL -------------- ---------------- MATRIX QC ---------------- LCS LCSD RPO RPD 115 IISD RPD RPD UNITS RESULT PQL FLG %REC FLG %REC FLG LCL UCL RPD UCL FLG %REC FLG %REC FLG LCL UCL RPD UCL FLG Batch 8260*9787123 Method 8260A - Volatile Organics, GCMS 1,1,1.2-Tetrachloroethane mg/kg 0 0 005 - 90 - - - 71 139 - 1,1,1-Trichloroethane mg/kg 0 0 005 - 103 - - - 70 135 - 1,1,2,2-Tetrachloroethane mg/kg 0 0 005 - 85 - - - 71 105 - 1,1,2-Trichloroethane mg/kg 0 0 005 - 97 - - - 68 133 _ 1,1-Dlchloroethane mg/kg 0 0 005 - 113 - - - 55 131 - 1,1-Dichloroethene mg/kg 0 0 005 - 113 - - - 58 13I - - - 102 - 118 - 61 142 14 35 1.1-Dichloropropene mg/kg 0 0 005 - 108 - - - 68 135 - - - - - - - - - _ _ _ 1,2,3-Trichlorobenzene mgJkg 0 0 005 - 81 - - - 62 139 - - 1,2,3-Trichloropropane mg/kg 0 0 005 - 69 - - - 49 132 - 1,2,4-Trichiorobenzene mg/kg 0 0 005 - 85 - - - 66 135 1.2.4-Trimethylbenzene mg/kg 0 0 005 - 106 - - - 78 128 1,2-Dibromo-3-chloropropane mg/kg 0 0 005 - 56 - - - 50 146 1,2-Dibromoethane mg/kg 0 0 005 - 81 - - - 64 140 1,2-Dichloroethane mg/kg 0 0 005 - 98 - - - 85 108 1,2-Dichlorobenzene mg/kg 0 0 005 - 92 - - - 73 128 - 1,2-Dichloropropane mg/kg 0 0 005 - 116 - - - 62 130 - 1,3,5-Trimethylbenzene mg/kg 0 0 005 - 109 - - - 75 131 - 1,3-Dichlorobenzene mg/kg 0 0 005 - 97 - - - 74 128 - 1,3-Dichloropropane mg/kg 0 0 005 - 100 - - - 74 125 - 1,4-Dichlorobenzene mg/kg 0 0 005 - 90 - - - 73 130 - 2,2-Dichloropropane mglkg 0 0 005 - 93 - - - 62 139 - 2-Chlorotoluene mg/kg 0 0 005 - 111 - - - 63 138 - 2-Hexanone mg/kg 0 0 05 - 55 - - - 23 166 - 4-Chlorotoluene mg/kg 0 0 005 - 113 - - - 67 139 - Acetone mg/kg 0 0 02 - 59 - - - 32 180 - Bromobenzene mg/kg 0 0 005 - 88 - - - 69 122 - Bromochloromethane mg/kg 0 0 005 - 98 - - - 72 129 - - - - Bromod7chloromethane mg/kg 0 0 005 - 96 - - - 67 134 - - - Bromomethane mg/kg 0 0 005 - 106 - - - 67 129 - - - Benzene mg/kg 0 0 005 - 115 - - - 76 123 - - - 112 - 119 - 73 129 6 36 - Bromoform mg/kg 0 0 005 - 67 - - - 61 148 - - - - - - - - - _ _ _ Chlorobenzene mg/kg O 0 005 - 102 - - - 70 140 - - - 101 - 103 - 67 146 2 38 Carbon Tetrachloride mg/kg 0 0 005 - 9D - - - 70 140 - - - - _ _ _ _ _ _ _ _ Chloroethane mg/kg 0 0 005 - 137 Q - - 54 135 - - - - - - - - - - - - Chloroform mg/kg 0 0 005 - 116 - - - 70 128 - - - Chloromethane mg/kg 0 0 005 - 96 - - - 40 136 - - - - - - - - - - - - Carbon Disulfide mg/kg 0 0 005 - 102 - - - 54 135 - - - - - - - - - - -