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Sequoia 680 Chesapeake Dnve Redwood City,CA 94063 (650) 364 9600 FAX(654)364-9233 <br /> (D 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX (916)921 0100 <br /> Cambria Client Prof ID Shell 2575 Country Club Blvd Sampled 12/15/97 ' <br /> 270 Perkins Ave Sample Descript MW-13-60 Received 12/19/97 <br /> Sonoma, CA 95476 Matrix SOLID <br /> Analysis Method 8015Mod/8020 Analyzed 12/23/97 <br />- Attention Joe Neely Lab Number 9712D12-01 _ Reported 12131197 „ <br /> QC Batch Number GC1223978020EXA µ <br /> Instrument ID GCHP01 <br /> Analyte Detection Limit Sample Results <br /> mg/Kg mg/Kg <br /> TPPH as Gas 10 N D <br /> Methyl t-Butyl Ether 0 025 N D <br /> Benzene 00050 N D <br /> Toluene 00050 N D <br /> Ethyl Benzene 00050 N D <br /> Xylenes (Total) 00050 N D <br /> Chromatogram Pattern <br /> Surrogates Control Limits% % Recovery <br /> Trifluorotoluene 70 130 82 <br /> 4-Bromofluorobenzene 60 140 Q <br /> is <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOIA ANALYTICAL - ELAP 01624 <br /> e 6regory <br /> Project Manager Page t <br />