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Sequoia 680 Chesapeake Lane <br /> Walnut City CA 94063 (650) 364 9600 FAX(650)364 9233 <br /> ID 444 iV Wiget Lane Walnut Crcek CA 44598 {510} 988 9600 FAX(510) 988 9673 <br /> IAnalytical 819 Sinker Avenue,Suite 8 Sacramento CA 95834 (416) 921 9600 FAX (916) 921 0100 <br /> Blaine Tech-Services Client Proi ID Shell Stockton/971202-L1 Sampled 12/02/97 <br /> 1680 Rogers Avenue Sample Descript MW-7 Received 12/03/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 12/09/97 <br /> Attention Fran Tiiie t:5l7 Number-971235&09 Reparted—12119197 <br /> QC Batch Number MS120997MTBEF3A <br /> Instrument ID F3 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Methyl t-Butyl Ether (MTBE) 20 32 <br /> Di-Isopropyl EtherDIPE) 20 N D <br /> Ethyl t-Butyl Ether (ETRE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 100 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SE7 AN ICAL - ELAP #1210 <br /> Peggy P er <br /> Project Manager Page 25 <br />