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Sequoia 680 Chesapeake Dnve Redwood City CA 94063 (650) 364 9600 FAX(650)364 9233 <br /> 4D 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510)988 %73 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Tech Services Client Proj ID Shell StocktW971202-1-1 Sampled 12/02/97 <br /> ' 1680 Rogers Avenue Sample Descript MW-11 Received 12/03/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 12/09/97 <br /> Attention Fran Thie Lab Number 9712360-13 Reported 12f 19f 97 <br /> QC Batch Number MS120997MTBEH6A <br /> Instrument ID H6 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Methyl t-Butyl Ether (MTBE) 20 N D <br /> Di-Isopropyl Ether (DIPE) 20 N D <br /> Ethyl t-Butyl Ether (ETBE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 104 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQ9nn LYTICAL - ELAP #1210 <br /> Project Manager Page 4 <br />