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Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (650) 364 9600 FAX(650)364-9233 <br /> 4D 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento, CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Tech Services - -Client Prod ID Shell Stockton/971222-F1 Sampled 12/22/97 - <br /> 1680 Rogers Avenue Sample Descript W-Down Received 12/23/97 <br /> r San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 12/30/97 <br />„ Attention Fran Thie Lab Number 9712F01-02 Reported 01JO7198 ; <br />-C Batch Number -MS123097MTBEH6A -- <br /> Instrument ID H6 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Methyl t-Butyl Ether (MTBE) 2.0 49 <br /> Di-Isopropyl Ether (DIPS) 20 N D <br /> Ethyl t-Butyl Ether(ETBE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> Surrogates Control Limits% % Recovery <br /> 1,2-Dichloroethane-d4 76 114 93 <br /> 0 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOI LYTICAL - ELAP #1210 <br /> gy Pe <br /> Project Manager Page 4 <br />