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Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (650) 364 9600 FAX(650)364 9233 <br /> (1) 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988-9600 FAX(510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Tech Services _ Client Prod ID Shell Stock-ton/971222-Fl _ Sampled 12/22/97 <br /> 1680 Rogers Avenue Sample Descnpt ES Received 12/23/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 12/31/97 <br /> Attention Fran Thie Lab Number 9712F01-08 Reported 01107198 <br /> DC Batch Number MS123097MTBEH6A <br /> nstrument ID H6 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Methyl t-Butyl Ether (MTBE) 20 N D <br /> Di-Isopropyl Ether (DIPS) 20 N D <br /> Ethyl t-Butyl Ether (EfBE) 20 D <br /> t-Amyl Methyl Ether (TAME) <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 97 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOI A YTICAL - ELAP #1210 <br /> y Pen e <br /> Project Man er Page 22 <br />