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Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (650) 364 9600 FAX(650)364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510) 988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Tech Services Client Prol ID Shell Stockton/970905-1`1 Sampled 09/05/97 <br /> 1680 Rogers Avenue Sample Descript Port 2452 C C Received 09/05/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 09/07/97 <br /> Attention Fran Thie Lab Number 9709144-01 Reported 09JO9197 <br /> DC Batch Number MS09079782601-16A <br /> Instrument ID H6 <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> n-Propylbenzene 20 N D <br /> Styrene 20 N D <br /> 1,1,1,2-Tetrachloroethane 20 N D <br /> 1,1,2,2-Tetrachloroethane 20 N D <br /> Tetrachloroethylene 20 N D <br /> Toluene 20 N D <br /> 1,2,3-Trlchlorobenzene 20 N D <br /> 1,2,4-Trlchlorobenzene 20 N D <br /> 1,1,1-Trichloroethane 20 N D <br /> 1,1,2-Trichloroethane 20 N D <br /> Trichloroethylene 20 N D <br /> Trichlorofluoromethane 20 N D <br /> Trlchloropropane 20 N D <br /> Trlmethylbenzene 20 N D <br /> 11 ,5-Trlmethylbenzene 20 N D <br /> Vinyl chloride 20 N D <br /> Total Xylenes 20 N D <br /> Surrogates Control Limits% % Recovery <br /> 1,2-Dichloroethane-d4 76 114 101 <br /> Toluene-d8 88 110 96 <br /> 4-Bromofluo robe nzene 86 115 104 <br /> Analytes reported as N were not present above the stated limit of detection <br /> SEQU A A YTICAL - ELAP #1210 <br /> Peggy nner <br /> Project Manager Page 2 <br />