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• Sequoia680 Chesapeake Drive Rcdwood City CA 94063 (650) 364 9600 FAX(650) 364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510) 988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916) 921 0100 <br /> Blaine Tech Services Client Prol ID Shell Stockton/970905-1`1 Sampled 09/05/97 <br /> 1680 Rogers Avenue Sample Descript Cal Trans Well #1 Received 09/05/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 09/06/97 <br /> Attention Fran Thie Lab Number 9709144-02 Reported 09109197 <br /> QC Batch Number MS090597MTBEH6A <br /> Instrument ID H6 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Metyl t-Butyl Ether(MTBE) 20 N D <br /> Di-Isopropyl Ether (DIPE) 20 N D <br /> Ethyl t-Butyl Ether (ETRE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 99 <br /> Analytes reported as ere not present above the stated limit of detection <br /> SEQU A ICAL - ELAP #1210 <br /> Peggy Pen <br /> Project Manager Page 8 <br />