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Alpha Analytical, Inc. <br /> n <br /> 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 • (775)355-0406 FAX • 1-800-283-1183 <br /> to OC Summary Report Fork Order <br /> Apr-OS 06032745 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D 1HPCHEMIMS091DATA1060328106032806 D Batch ID MS09W0328A Analysis Date 03/28/2006 10 39 <br /> Sample ID MBLK MS09W0328A Units pg/L Run ID MSD_09_060328A Prep Date 03/28/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REG Lowl-imit HighLimo#RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 10 <br /> Methyl tert-butyl ether(MTBE) ND 0 5 <br /> Di-isopropyl Ether(DIPS) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> 1,2-Dichloroethane ND i <br /> Benzene ND 0 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0 5 <br /> Ethylbenzene ND 05 <br /> m p-Xylene ND 0 5 <br /> o-Xylene ND 05 <br /> Surr 1 2-Dichloroethane-d4 10 10 100 76 127 <br /> Surr Toluene-d8 945 10 95 84 113 <br /> Surr 4-Bromofluorobenzene 978 10 98 79 119 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEMIMS091DATA1060328106032804 D Batch ID MS09W0328A Analysis Date 03/28/2006 09 52 <br /> Sample 1D LCS MS09W0328A Units pg/L Run ID MSD_09_060328A Prep Date 03/28/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 111 0 5 10 111 81 122 <br /> Toluene 102 05 10 102 80 120 <br /> Ethylbenzene 995 05 10 100 80 120 <br /> wm Xylene 109 05 10 109 80 129 <br /> ne 997 0 5 10 997 80 129 <br /> 1,2-Dichloroethane-d4 109 10 109 76 127 <br /> Surr Toluene-d8 941 10 94 84 113 <br /> Surr 4-Bromofluorobenzene 981 10 98 79 119 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D lf-IPCHEMIMS091OATA1060328106032812 D Batch ID MS09W0328A Analysis Date 03/28/2006 13 00 <br /> Sample ID 06032745-02AMS Units pg/L Run ID MSD_09_060328A Prep Date 03/28/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Benzene 519 1 3 50 0 104 74 125 <br /> Toluene 473 1 3 50 0 95 76 120 <br /> Ethylbenzene 458 1 3 50 0 92 77 124 <br /> m,p-Xylene 51 13 50 0 102 73 130 <br /> o-Xylene 469 1 3 50 0 94 74 131 <br /> Surr 1 2-Dichloroethane-d4 539 50 108 76 127 <br /> Surr-Toluene-d8 47 50 94 84 113 <br /> Surr 4-Bromofluorobenzene 491 50 98 79 119 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW82608 <br /> File ID D 1HPCHEMWIS091DATA\060328106032813 D Batch ID MS09W0328A Analysis Date 03/28/2006 13 23 <br /> Sample ID 06032745-02AMSD Units Ng/L Run ID MSD_09_060328A Prep Date 03/28/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hight-imit RPDRefVal %RPD(Limit) Qual <br /> Benzene 525 1 3 50 0 105 74 125 51 87 1 203) <br /> Toluene 48 1 3 50 0 96 76 120 4733 1 4(13) <br /> Ethylbenzene 465 1 3 50 0 93 77 124 4578 1 5(13) <br /> m,p-Xylene 521 1 3 50 0 104 73 130 5101 2 0(14) <br /> o-Xylene 474 1 3 50 0 95 74 131 469 1 103) <br /> Surr 1,2-Dichloroethane-d4 542 50 108 76 127 <br /> Surr Toluene-d8 469 50 94 84 113 <br /> Surr 4-Bromofluorobenzene 488 50 98 79 119 <br />