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A <br /> Alpha Analytical, Inc. <br /> 255 Glendale Ave -Suite 21 -Sparks,Nevada 89431-5778 <br /> (775)355-1044-(775)355-0406 FAX- 1-800-283-1183 <br /> Work Order <br /> Date OC Summary Report 05092906 <br /> 06-ori 0s <br /> Method Blank Type MBLK Test Code EPA Method SW8260B-0I <br /> File ID C IHPCHEM1MS111DATA1050930105093003 D Batch ID 13218 Analysis Date 0913012005 09 47 <br /> Sample tD MBLK-13218 Units pg1L Run ID MSD 11_050930A Prep Date 09130/2005 <br /> Analyte Result PQL SpkVal SpkReNal %REC LowLimit HighUrnit RPDRefVal %RPD(Limit) Qual <br /> Methanol ND 5000 <br /> Ethanol ND 5000 <br /> Surr Hexanuoro-2-propanol 517 500 103 63 13T <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B-DI <br /> File ID C 1HPCHEMMSIIIDATA1050930105093004 D Batch ID 13218 Analysis Date 0913012005 10 07 <br /> Sample ID LCS-13218 Units pg1L Run ID MSD 11 050930A Prep Hate 09/3012005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imd Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Methanol 253 50 250 101 45 155 <br /> Ethanol 245 5 250 98 51 144 <br /> Surr Hexafluoro-2-propanol 503 500 101 63 137 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B-0I <br /> File ID C IHPCHEMXMsil1DATA1050930105093006 D Batch ID 13218 Analysis Date 09130/200510 48 <br /> Sample ID 05092262-02AMS Units pg1L Run ID MSD 11050930A Prep Date 09/3012005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDReNal %RPD(Limit) Qual <br /> Methanol 266 50 250 0 107 45 163 <br /> 7 50 149 <br /> Ethanol 242 5 25 0 gg 7 63 137 <br /> Surr Hexafluoro-2-propanol 499 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B-DI <br /> Batch ID 13218 Analysis Date 091301200511 08 <br /> File ID C IHPCHEM1MS111DATA1050930105093007 D prop pate 09/3012005 <br /> Sample ID 05092262-02AMSD Units pg1L Run ID MSD 11050930A <br /> alResult PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit)Qual <br /> yte <br /> ethanol 271 50 250 0 108 45 163 2663 1 8(22) <br /> 254 5 250 0 101 50 149 2422 4 6(15) <br /> Ethanol <br /> Surr Hexafluoro-2-propanol <br /> 514 500 103 63 137 <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However for reponing purposes,all QC data is rounded to three significant figures Therefore hand calculate <br /> values may differ slightly <br /> Reported in nnerograms per titer per client request <br />