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JIr64 <br /> S 1455 McDowell Blvd North Ste D <br /> equola Petaluma CA 94954 <br /> Analytical (707) 792 1865 <br /> FAX f707) 792 0342 <br /> lta Erivironmental Consultants Project Exxon Sampled 5/26/99 <br /> Gold Camp Dr, Suite 200 Project Number 7-3708/D093-S09 IzPr�, rai ;traron <br /> Rancho Cordova C4 95670 Project Manager Jim Brownell Reported 6/21/99 <br /> 'volatile Organti- Compounds by EPA Nlethod 8260B,Qualttti Control <br /> Sequoia Analvttcal -Petaluma <br /> Date Spike Sample QC Reporttag Limit Recon RPD RPD <br /> nalyrte analyzed Level Result Result Units Recov Limits % Limit % Notes' <br /> CS 9060258-BS2 <br /> ethyl tert-butyl ether 6/9/99 500 53 5 uglhg 75 8-124 107 <br /> Surrogate Dt6romofluotomethane 50 0 52 3 800-120 105 <br /> urrogate 1 2 Drcliloroetlrane d4 50 0 56 5 860-120 113 <br /> W, Toluene d8 50 0 51 6 81 0-117 103 <br /> arrogate 4 Bromofluoroben_ene 50 0 )1 7 740-121 103 <br /> CS 9060358-BS3 <br /> 111�et_hvl tent-butyl ether _ 6/9/99 500 _ 54 5 ug,kg _75 8-124 _ 109 <br /> Surrogate Dtbromofluornmetharte 50 0 52 0 800-120 104 <br /> urra�att 1 2-Drchloroethane-d4 500 53 3 800-120 107 <br /> arrogate Coluene d8 50 0 )1 8 810 1// 104 <br /> urrogate 4 Bromofluoroben:ene 500 52 8 740-121 106 <br /> atrtx S tke 9060358-N(SI P906019-10 <br /> hyl tert-butyl ether_ 6,8/99 _ 500_ ND_ 59 5 ig k 75 8-124 1 E9 <br /> rrogate Dtbrom-Jill ronrethane <br /> 500 53 7 800-120 107 <br /> Ourrogate 12-Drchloroethane, d-1 -)00 518 800-110 116 <br /> urrogate Toluene d8 500 53 ? 81 0-117 106 <br /> urrogate 4 Bramofluoroben:ene 50V 5-1 7 74 0421 109 <br /> atrtc Spike Du 9060258-NISDI P906019-10 <br /> ethyl tent--butyl ether _ 6/9199 _ 500 _ _ N_ D_ 58 I ug/kg 75 3-124 116 35 0 _3 5_5 <br /> urrogate Dt6romofluoromethane 500 54 1 800-120 108 f <br /> trrogale 1 2 Drchloroethane-d4 500 579 800-120 116 <br /> rrogate Toluene-d8 500 546 81 0-117 109 <br /> rrogate 4-Bromofuoroben�ene 500 561 740-121 112 <br /> quota Analytical -Petaluma *Refer ro end ofrepart for next of notes and defintttons <br />' Page 17 of 19 <br />