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Report Number 46282 QC Report Matrix Spike/Matrix Spike Duplicate Date 10/10/2005 Project Name 7-Eleven Store#14117 Project Number 77EL.14117.05 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 46261-03 <0 50 392 400 380 38 6 ug/L EPA 8260B 1016105 96 8 966 0 273 70-130 25 Toluene 46261-03 <0 50 392 400 372 378 uglL EPA 8260B 1016105 949 94 4 0 506 70-130 25 Tert-Butanol 46261-03 <5 0 196 200 197 197 uglL EPA 8260B 10/6105 100 987 175 70-130 25 Methyl-t-Butyl Ether 46261-03 <0 50 39 2 400 381 394 uglL EPA 82608 10/6105 971 985 1 36 70-130 25 Benzene 46284-06 <0 50 400 400 377 371 uglL EPA 8260B 1015105 94 2 92 8 1 50 70-130 25 Toluene 46284-06 <0 50 400 400 36 5 35 7 uglL EPA 8260B 1015105 912 89 3 209 70-130 25 Tert-Butanol 46284-06 <5 0 200 200 204 204 ug/L EPA 8260B 1015105 102 102 0202 70-130 25 Methyl-t-Butyl Ether 46284-06 130 400 400 162 159 uglL EPA 8260B 1015105 872 786 103 70-130 25 Benzene 46282-08 120 400 400 160 152 ug/L. EPA 8260E 1015105 889 71 1 223 70-130 25 Toluene 46282-08 220 400 400 264 256 uglL EPA 82606 1015105 105 827 236 70-130 25 Tert-Butanol 46282-08 170 200 200 378 376 uglL EPA 8260B 1015105 102 101 0 859 70-130 25 Methyl-t-Butyl Ether46282-08 190 400 400 225 217 ug/L EPA 8260B 1015105 971 775 224 70-130 25 Benzene 46284-03 21 400 400 408 402 ug/L EPA 8260B 1015105 966 951 162 70-130 25 Toluene 46284-03 <0 50 400 400 378 377 ug1L EPA 82606 1015105 94 5 94 3 0 257 70-130 25 Tert-Butanol 46284-03 <5 0 200 200 195 199 uglL EPA 8260B 1015105 97 7 996 187 70-130 25 Methyl-t-Butyl Ether 46284-03 0 59 400 400 449 447 uglL EPA 82606 1015105 111 110 0 501 70-130 25 )94' KIFF ANALYTICAL, LLC Approved By Jo iff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800