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s s i Report Number 44602 QC Report Matrix Spike/Matrix Spike Duplicate Date 7/6/2005 Protect Name 7-Eleven Store#14117 Protect Number 77EL.14117.05 Siked Duplicate Spiked Spiked to Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 44602-01 <0 50 400 400 402 39 3 ug/L EPA 8260B 711105 100 982 2 33 70-130 25 Toluene 44602-01 <0 50 400 400 402 39 7 ug/L EPA 8260B 711105 100 99 3 122 70-130 25 Tert-Butanol 44602-01 16 200 200 232 228 ug/L EPA 8260B 711105 108 106 165 70-130 25 Methyl-t-Butyl Ether44602-01 <0 50 400 400 352 354 ug/L EPA 8260B 719105 879 88 4 0 583 70-130 25 Benzene 44575-06 <0 50 400 400 401 398 ug1L EPA 8260B 711105 100 99 6 0 574 70-130 25 i Toluene 44575-06 <0 50 400 400 437 433 ug/L EPA 8260B 711105 109 108 106 70-130 25 Tert-Butanol 44575-06 <50 200 200 220 220 ug/L EPA 8260B 711105 110 110 0 198 70-130 25 Methyl-t-Butyl Ether44575-06 <0 50 400 400 385 381 ug/L EPA 8260B 711105 962 952 1 15 70-130 25 Benzene 44619-01 <0 50 400 400 406 394 ug/L EPA 8260B 715105 101 984 308 70-130 25 Toluene 44619-01 <0 50 400 400 442 426 ug/L EPA 8260B 715105 110 106 373 70-130 25 Tert-Butanol 44619-01 21 200 200 244 247 ug/L EPA 8260E 715105 111 113 127 70-130 25 Methyl-t-Butyl Ether44619-01 28 400 400 673 662 ug/L EPA 82608 715105 977 952 266 70-130 25 Benzene 44583-03 <0 50 400 400 406 404 ug/L EPA 8260B 711105 101 101 0 460 70-130 25 Toluene 44583-03 <0 50 400 400 409 405 ug/L EPA 8260B 711105 102 101 0 952 70-130 25 Tert-Butanol 44583-03 <5 0 200 200 196 196 ug/L EPA 8260B 711105 980 98 0 0 00446 70-130 25 Methyl-t-Butyl Ether44583-03 <0 50 400 400 367 365 ug/L EPA 8260B 711105 91 8 912 0 680 70-130 25 Approved By Jo iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800