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110 2nd Avenue South,4137 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925 758 1620 Fax 925-798 1622 <br /> http l/www mccampbell corn E mail m in@mccampbell com <br /> I T Corporation Client Project ID #20632,STHL/Stockton Date Sampled 04/10/02 <br /> 4005 Port Chicago Hwy Date Received 04/10/02 <br /> Client Contact Shelby Lathrop Date Extracted 04/17/02 <br /> Concord, CA 94553-2233 <br /> Client P O Date Analyzed 04/17/02 <br /> Oxygenated Volatile Organics by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0204212 <br /> aLab ID 0204212-OOIB 0204212-002B 0204212-003B� 0204212-004B <br /> Client ID MW-6 MW-7 MW-4R MW-2 Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF 1 1000 1000 120 S W <br /> Compound Concentration ug/kg µg/L <br /> Diisopropyl ether(DIPE) ND ND<500 ND<500 ND<62 NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND<500 ND<500 ND<62 NA 05 <br /> Methyl-t-butyl ether(MTBE) 1 1 22000 1 5900 1900 — NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND<500 N13<500 i ND<62 NA 05 <br /> rMARIN <br /> ---- f -- -- — -- -- — <br /> t-Butyl alcohol(TBA) ND ND<5000 230000 ND<620 NA 5 <br /> Surrogate Recoveries(%} <br /> Dibromofluoromethane 994Z_ 865 111 978 <br /> E <br /> Comments <br /> *water samples are reported in ug IL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP!STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present,(t)liquid sample that contains greater than–2 vol %sediment,0)sampie diiuted due to high <br /> norganic content <br /> U <br /> U <br /> D <br /> 0 aiiiN <br /> D <br /> DHS Certification No 1644 Edward Hairulton,Lab Director <br /> U <br />