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FLUOR DANIEL GTI, INC <br /> STANDARD OPERATING PROCEDURE <br /> CONCERNING SOIL SAMPLING METHODOLOGY <br /> SOP 14 <br /> 1 Soil samples should be collected and preserved in accordance with Groundwater Technology <br /> Standard Operating Procedure (SOP 15) concerning Soil Sample Collection and Handling when <br /> Sampling for Volatile Organics A hollow stem soil auger should be used to drill to the desired <br /> sampling depth A standard 2 inch diameter split spoon sampler 18 inches in length shall be used to <br /> collect the samples The samples are contained to 2 inch diameter by 6 inch long thin walled brass <br /> tube liners fitted into the split spoon sampler(three per sampler) <br /> 2 The split spoon sampler should be driven the full depth of the spoon into the soil by a 140 pound <br /> hammer The spoon shall then be extracted from the borehole and the brass tube liners containing <br /> the sod sample removed from the sampler The ends of the liner tubes should be immediately covered <br /> with aluminum foil, sealed with a teflon or plastic cap, and taped with duct tape After being properly <br /> identified with sample data entered on a standard chain of custody form the samples shall be placed <br /> on dry ice (maintained below 4—C) and transported to the laboratory within 24 hours <br /> 3 One of the three soil samples retrieved at each sample depth shall be analyzed in the field using a <br /> photoionization detector and/or explosimeter The purpose of the field analysis is to provide a means <br /> to choose samples to be laboratory analyzed for hydrocarbon concentrations and to enable <br /> comparisons between the field and laboratory analyses The soil sample shall be sealed in a plastic <br /> bag and allowed to equilibrate with the air surrounding the soil for approximately 10 minutes One of <br /> the two field vapor instruments shall be used to quantify the amount of hydrocarbon released to the <br /> air from the soils The data shall be recorded on the drill logs at the depth corresponding to the <br /> sample point <br />