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SURROGATE RECOVER I ES REPORT Report Date 02/18/2000 Job Number 200278 ;;] CUSTOMER IT Group PROJECT- Southland - Martinez ATTN Rhonda Teicheira Method Volatile Orgam cs by GC/Ms Batch 11004 Method Code 82600X Analyst gfb Surrogate Units Dibromofluoromethane ug/L Lab ID Matrix OC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 200240-2 Liquids 1 25 99 25 000 104 0 57-162 02/01/2000 1627 200240-2 Liquids MS 26 26 25 000 105 0 57-162 02/01/2000 2013 25 000 101.6 57-162 02/01/2000 2041 200240-2 Liquids MSD 25 40 25 000 93 3 60-160 02/04/2000 0502 200262-21 Solid 1 23 33 200262-21 Solid M5 23 52 25 000 94 1 60-160 02/04/2000 0914 200262 21 Solid MSD 23 28 25 000 93.1 60-160 02/04/2000 0945 200271-9 Liquids 2000 22 00 25 000 88 0 57-162 02/09/2000 0128 LCS 1 22 51 25 000 90 0 57-162 02/09/2000 0201 200271-10 Liquids 1000 22 62 25 000 90 5 57-162 02/09/2000 0236 200277-2 Liquids 20 22 36 25 000 89.4 57-162 02/09/2000 0307 280-1 Liquids 50 21 47 25 000 85 9 57-162 02/09/2000 0339 0-2 Liquids 100 22 10 25 000 88 4 57-162 02/09/2000 0410 NW80-3 Liquids 1 21 91 25 000 87.6 57-162 02/09/2000 0441 200281-1 Liquids 1 21 56 25 000 86 2 57-162 02/09/2000 0512 200278-1 Liquids 1 21 75 25 000 87 0 57-162 02/09/2000 0545 200278-2 Liquids 2 22 27 25 000 89.1 57-162 02/09/2000 0616 200278-3 Liquids 1 21 79 25 000 87 2 57 162 02/09/2000 0648 200278-4 Liquids 1 22 02 25 000 88 1 57-162 02/09/2000 0719 200279-1 Liquids 1 22 63 25 000 90 5 57-162 02/09/2000 0750 200279-2 Liquids 1 22 16 25 000 88 6 57-162 02/09/2000 0820 200279-3 Liquids 25 21 73 25 000 86 9 57-162 02/09/2000 0852 MB 1 22 39 25 000 89 6 57-162 02/09/2000 1040 200262-16 Solid 1 25 20 25 000 100 8 60-160 02/09/2000 1113 200262-5 Solid 5 22 12 25 000 88 5 60-160 02/09/2000 1147 Method Volatile Organics -Aromatics Batch 11018 Method Code 8020BX Analyst evd Surrogate Units 4-Bromofluorobenzene ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time CV 1 37 50 50 0000 75 0 64-147 02/10/2000 1129 MB 1 37 10 50 0000 74 2 64-147 02/10/2000 1154 LCS 1 37 32 50 0000 74 6 64-147 02/10/2000 1312 LCD 1 37 50 50 0000 75 0 64-147 02/10/2000 1338 200277-4 Liquids 10 36 79 50 0000 — — 73 6 64-147 02/10/2000 1436 200295-1 Liquids 50 38 92 50 0000 77 8 64-147 02/10/2000 1522 MB 1 37 69 50 0000 75 4 64-147 02/10/2000 1547 299-1 Liquids 1 37 53 50 0000 75 1 64-147 02/10/2000 1613 78-1 Liquids 1 35 13 50 0000 70 3 64-147 02/10/2000 1639 99-4 Liquids 1 34 67 50 0000 69 3 64-147 02/10/2000 1756 200299-5 Liquids 10 34 77 50 0000 69 5 64-147 02/10/2000 1822 Page 16