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C01,1LAB CORE LABORATORIES <br /> D U A L I T Y A S S U R A N C E F 0 0 T E R <br /> METHOD REFERENCES <br /> (1) EPA Sw-846, Test Methods for Evaluating Solid baste, Third Edition, September 1986, and Updates I, II, IIA, IIB, and III <br /> (2) Standard Methods for the Examination of Water and Wastewater, 18th Edition, 1992 <br /> (3) EPA 600/4-79-020, Methods of Chemical Analysis for Waters and Wastes, March 1983 <br /> (4) Federal Register, Friday, October 26, 1984 (40 CFR Part 136) <br /> (5) American Society for Testing and Materials, Volumes 5 01, 5 02, 5 03, 1992 <br /> (6) EPA 600/4-89-001, Short-term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Fresh <br /> Water Organisms <br /> (7) EPA 600/4-90-027, Methods for Measuring the Acute Toxicity of Effluent and Receiving Waters to Fresh Water and Marine <br /> Organisms, Fourth Edition <br /> COMMENTS <br /> All methods of chemical analysis have a statistical uncertainty associated with the results. Unless otherwise indicated, <br /> the data in this report are within the limits of uncertainty as specified in the referenced method Quality control <br /> acceptance criteria are based either on limits specified in the referenced method or on actual laboratory performance <br /> The date and time of analysis indicated on the QC report may not reflect the actual time of analysis for QC samples Data <br /> reported in the QA report may be lower than sample data due to dilution of samples into the calibration range of the analysis <br /> Sample concentrations for solid samples are calculated on an as received (wet) basis unless otherwise indicated Unless <br /> otherwise indicated, volatiles by gas chromatography (GC) are reported from a single column Volatiles analyses by GC on low <br /> Level soils are conducted at room temperature TCLP extractions are performed at sample amounts, approved by the State of <br /> California <br /> LAGS, FOOTNOTES, AND ABBREVIATIONS (as needed) <br /> NA = Not analyzed N.I = Not Ignitable <br /> N/A = Not applicable S.I. = Sustains Ignition <br /> ug/L = Micrograms per liter I(NS) = Ignites, but does not Sustain Ignition <br /> mg/L = Milligrams per liter RPD = Relative Percent Difference <br /> ND = Not detected at a value greater than the reporting limit <br /> NC = Not calculable due to values lower than the detection limit <br /> (a) = Surrogate recoveries were outside acceptable ranges due to matrix effects <br /> (b) = Surrogate recoveries were not calculated due to dilution of the sample below the detectable range for the surrogate. <br /> (c) = Matrix spike recoveries were outside acceptable ranges due to matrix effects <br /> (d) = Relative Percent Difference (RPD) for duplicate analysis outside acceptance limits due to actual differences in <br /> the sample matrix. <br /> (e) = The limit listed for flammability indicates the upper limit for the test. Samples are not tested at temperatures <br /> above 140 Fahrenheit since only samples which will sustain ignition at temperatures below 140 are considered <br /> flammable. <br /> (f) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern Results were quantified using a <br /> diesel standard, however, the hydrocarbon pattern did not match a diesel pattern. <br /> (g) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern Results were quantified using a <br /> gasoline standard, however, the hydrocarbon pattern did not match a gasoline pattern. <br /> (h) = High dilution due to matrix effects <br /> CC SAMPLE IDENTIFICATIONS SUBCONTRACTED LABORATORY LOCATIONS <br /> MB = Method Blank SS = Storage Blank Core Laboratories: Aurora, Colorado *AU <br /> RB = Reagent Blank MS = Matrix Spike Casper, Wyoming *CA <br /> ICS = Initial Calibration Stank MSD = Matrix Spike Duplicate Corpus Christi, Texas *CC <br /> CCS = Continuing Calibration Blank MD = Matrix Duplicate Edison, New Jersey *ED <br /> CS = Calibration Standard BS = Blank Spike Houston, Texas (Env) *HE <br /> ICY = Initial Calibration SS = Surrogate Spike Houston, Texas (Pet) *HP <br /> Verification LCS = Laboratory Control Indianapolis, Indiana *IN <br /> CCV = Continuing Calibration Standard Lake Charles, Louisiana *LC <br /> Verification RS = Reference Standard Long Beach, California *LB <br /> Valparaiso, Indiana *VP <br /> Bakersfield, California *BK <br /> 1250 Gene Autry Way Autry Way <br /> Anaheim, CA 92805 <br /> (714) 937-1094 /u/batt/Logs n forms/footer form <br /> Tin'aNsyb-aeuba W—ns a nlarpralBildri ppnt8 nod In Ihs ropod—basstl upon lnbrmefwn add fnalnuf supp4etl by the Ulanr for wtgso ae[1p anp opntganl at use Ihla repo"has been made The enalyt Wi r sJM opbtlona a mrarpeta Irons <br /> a IXassad ral}e6an1 the bast jWg—W Ctrs L-W-1-1 CIX. Mwave makas no xrarrinty P raprasantel m 11pr95a or Impl ad pl ern/type and expr9asf,'d6olaima>Same as t.the p.0uG vity pri,W bperat—M prolrtebleneaa of <br /> any oa Das C0 or otna onaral prpparty was o santl In con—i,n with con SWn repel la aaab d rglso upas for any mesal whatapevar This report shall not be raproducad 0 wide w In peri without the written approval el Cwa uowaVfneII <br />