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Canonie Environmental Case Narrative <br /> Client : ENVIRONMENTAL SOLUTIONS Project t:L90076 <br /> LP # : 9838 <br /> Inorganics Case Narrative <br /> Analysis completed in accordance with methods cited. <br /> Volatiles Case Narrative <br /> Calibration was verified for all samples analyzed. <br /> Surrogate recoveries were within acceptable limits . <br /> The method blank associated wa.th this group of samples was <br /> free from target analyte interferences at, or above, the <br /> reporting limits. <br /> Spike recoveries were within acceptable limxts . <br /> pesticides Case Narrative <br /> TEH: Calrbratzon was verified for all samples analyzed_ The <br /> Method Blank was free from interferences at or above the <br /> reporting limits. Interferences in sample ST-2A (855177) <br /> exceeded the spike concentration and required a dilution for <br /> analysis which qualifies any recovery data. Sample 26000 <br /> GAL STOCK PILE (855184) contained petroleum hydrocarbons <br /> that were below the reporting limit at a concentration of <br /> 0 - 712 ppm- <br /> FUM: Calibration was verified for all samples analyzed_ The <br /> method blank was free from interferences at or above the . <br /> reporting limits- Spike and spike duplicate recoveries were <br /> within acceptable limits. <br /> Extractions Pest. Case Narrative <br /> E504-5/FUMIGANT <br /> All samples were extracted within required holding time by <br /> Canonie shake-down method for fumigant extraction. The <br /> final volume for all the extracts was 5. 0 ml - <br /> ETEH-S <br /> All samples were extracted within required holding time by <br /> .method 3550. The final volume of all the extracts was 2 . 0 <br /> ml . <br /> • <br /> CanonieEnvironmental <br />