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' Alpha Analytical, Inc. <br /> Q 255 Glendale Ave Suite 21 •Sparks, Nevada 89431-5778 <br /> (775)355-1044•(775) 355-0406 FAX• 1-800-283-1183 <br /> Date QC Summary Report 04102 <br /> 1G Not 04 0410224433 <br /> Method Blank Type MBLK Test Code EPA Method SW6020 <br /> File ID 110304 81220A_IC13 D Batch ID 11041 Analysis Date 11/04/2004 03 19 <br /> Sample ID MB-19041 Units mg/t. Run ID ICPIMS 0411038 Prep Date 11104/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUrnit HighLimit RPDReNal %RPD(Limit) Qual <br /> Chromium ND 0 005 <br /> Manganese ND 001 <br /> Copper ND 001 <br /> Zinc ND 01 <br /> Arsenic ND 0 005 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW6020 <br />' File ID 110304 W221A_LCS D Batch ID 11041 Analysis Date 11/04/2004 03 23 <br /> Sample ID LCS-11041 Units mglL Run ID ICPIMS 0411038 Prep Date 11/02/2004 <br /> I <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDReIVaE %RPD(Limit) Qual <br /> I <br /> Chromium 0 249 0 005 025 996 85 115 <br /> Manganese 259 001 2 5 104 85 115 <br /> Copper 0 266 0 01 025 106 85 115 <br /> Zinc 0 263 01 025 105 85 115 <br /> Arsenic 0 263 0 005 025 105 85 115 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW6020 <br /> File ID 110304 B1224SMPL D1 Batch ID 11041 Analysis Date 11/04/2004 03 36 <br /> Sample ID 04102743-01AMS Units mglL Run ID ICPIMS-041103B Prep Date 11/0212004 <br />' Analylo Result PQL SpkVal SpkReNal %REC LowLimit HighLimit RPDRetVal %RPD(Limit) Qual <br /> Chromium 0 246 0 005 025 0 98 70 130 <br /> Manganese 272 001 25 0 1601 102 70 130 <br /> Copper 0 262 001 0 25 0 105 70 130 <br /> Zinc 0 304 01 0 25 0 122 70 130 <br /> Arsenic 0 263 0 005 025 0 105 70 130 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW6020 <br />' File 10 110304 B1225SMPL DI Batch ID 11041 Analysis Date 11104/2004 03 40 <br /> Sample ID 04102743-01AMSD Units mg1L Run lD ICPIMS 0411038 Prep Date 11102/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUrnit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Chromium 025 0 005 025 0 100 70 130 02457 1 9(20) <br /> Manganese 275 0 01 25 01601 103 70 130 2 719 1 0(20) <br /> Copper 0 265 0 01 025 0 106 70 130 02619 1 3(20) <br /> Zinc 0 309 01 025 0 123 70 130 03041 1 5(20) <br /> Arsenic 0 269 0 005 025 0 108 70 130 02634 2 1(20) <br /> Comments <br /> Calculations arc based off of raw(non-rounded)data However For reporting purposes all QC data is rounded to three significant figures Therefore,hand calculated <br /> i values may differ slightly <br /> 1 <br />