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' Alpha Analytical, Inc, <br /> 255 Glendale Ave • Suite 21 -Sparks, Nevada 89431-5778 <br /> (775)355-1044 -(775)355-0406 FAX - 1-800-283-1183 <br /> Date <br /> 16 rYoti-174 <br /> QC Summary Report Work Order <br /> 04102243 <br /> Method Blank Type MBLK Test Cade EPA Method SW6020 i <br /> Fde ID 110304 B1021A_ICB D Batch 10 11013 Analysis Date 11103/2004 13 18 <br /> Sample ID MB-11013 Units mg/Kg Run ID' ICP/MS_041103A Prep Date 11103/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imn RPDReNaI %RPD(Limtl) Qual <br /> Chromium ND 1 <br /> Manqanese NO 2 <br /> Iron NO 500 <br />' Copper NO 2 <br /> Zinc ND 20 <br /> Arsenic ND 1 <br />' Laboratory Control Spike Type LCS Test Code EPA Method SW6020 <br /> File ID 110304 B1314 LCS Dl Batch ID 11013 Analysts Date 11/04/2004 10 05 <br /> Sample ID LCS-11013 Units mg/Kg Run ID ICP/MS O41103A Prep Date 1012812004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Htght_imit RPDRefVal %RPD(Limit) Qual <br />' Chromium 243 1 25 97 85 115 <br /> Manganese 259 2 250 104 85 115 <br /> Iron 4920 500 5000 98 85 115 <br /> r Copper 25 7 2 25 103 85 115 <br />'t Zinc 261 20 25 104 85 115 <br /> Arsenic 255 1 25 102 85 115 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW6020 <br /> Fite ID 110304 81025MS DI Batch ID 11013 Analysis Date 11/03/2004 13 35 <br />' Sample ID 04102601-06AMS Units mg1Kg Run ID ICPIMS_041103A Prep Date 11103/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUnnit Hight-trait RPDReNaI %RPD(Ltmit) Qua? <br /> Chromium 372 1 25 1032 107 70 130 <br /> Manganese 421 2 250 1461 110 70 130 <br /> Iron 15100 500 5000 9620 110 70 130 <br /> Copper 332 2 25 5 263 112 70 130 <br /> Zinc 51 9 20 25 2554 106 70 130 <br /> Arsenic 281 1 25 1214 108 70 130 <br /> it Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW6020 <br /> Fife 10 110304 81026MSD Dl Batch ID 11013 Analysis Date 11/03/2004 13 39 <br /> Sample ID 04102601-05AMSO Units mg/Kg RunID ICP/MS_041103A Prep Date 11/03/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLtmit RPORefVal %RPD(Limit) Qual <br /> Chromium 38 7 1 25 1032 114 70 130 3715 4 1(20) <br /> Manganese 428 2 250 1461 113 70 130 4206 1 8(20) <br /> Iron 15500 500 5000 9620 118 70 130 15120 2 6(20) <br />' Copper 356 2 25 5 263 122 70 130 33 21 7 1(20) <br /> Zinc 54 4 20 25 2554 116 70 130 5194 4 7(20) <br /> Arsenic 305 1 25 1 214 117 70 130 28 1 B 1(20) <br /> Comments <br /> Calculations are based off of raw(non-rounded)data Ho%kever for reporting purposes all QC data is rounded to three significant figures Therefore hand calculated <br /> values may differ slightly <br /> I <br /> i <br />