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Alpha Analytical, Inc. <br /> 255 Glendale Ave - Suite 21 -Sparks Nevada 89431-5778 <br /> 4A (775) 355-1044 - (775) 355-0406 FAX- 1-800-283-1183 <br /> Dote 14ork order <br /> 16 nfou 04 OC Summary Report <br /> il4lo»s, <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID C 1HPCHEM1MS071DATA1041027104102719 D Batch 0 MS07SO989A Analysis Date 10127/2004 14 07 <br /> Sample ID MBLK MS07SO989A Units jig/Kg Run IO MSO_07_041027A Prep Date 10/2712004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPDRefVal %aRPD(Limit) Qual <br /> Chloromethane NO 40 <br /> Vinyl chloride NO 20 <br /> I Chloroethane NO 20 <br /> Bromomethane <br /> NO 40 <br /> Tnchlorofluoromethane NO 20 <br /> 11-Dichloroethene NO 20 <br /> Dichloramelhane NO 40 <br /> trans-12-Dtchloroethene ND 20 <br /> 1,1-Dichlomethane NO 20 <br /> cis-l2-Dtchloroethene NO 20 <br /> Chloroform NO 20 <br /> 12-Dichloroethane NO 20 <br /> 11 1-Tnchloroethane ND 20 <br /> Carbon tetrachloride ND 20 <br /> Benzene ND 5 <br /> 12-Dichloropropane ND 20 <br /> Tnchloroethene ND 20 <br /> Bromodichloromethane ND 20 <br /> as-13-Dichloropropene ND 20 <br /> trans-t 3-Dichloropropene ND 20 <br /> 11 2-Tnchloroethane ND 20 <br /> Toluene NO 5 <br /> Dibromochloromethane ND 20 <br /> Tetrachloroethene NO 20 <br /> •Chlorobenzene NO 20 <br /> Ethylbenzene NO 5 <br /> m p-Xylene ND 5 <br /> Bromoform NO 20 <br /> o-Xylene NO 5 <br /> 1 1 2 2-Tetrachloroethane ND 20 <br /> 13-Dichlorobenzene NO 20 <br />{ 14-Dichlorobenzene NO 20 <br /> 12-Dichlorobenzene ND 20 <br /> Surr 1 2-Dichloroethane-d4 183 200 92 70 120 <br /> Surr Toluene-d8 205 200 102 79 124 <br /> Surr 4-Bromefluorobenzene 191 209 96 75 122 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW02608 <br /> File ID C%HPCHEM%MS071DATA1041027104102720 D Batch ID MS07SO989A Analysis Date 10/27/2004 14 29 <br /> Sample ID LCS MS07SO989A Units pg/Kg Run ID MSD_07_041027A Prep Date 10/27/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighUmit RPDRefVai %RPO(Limit) Quat <br /> 11-Dichloroethene 211 20 200 106 0 147 <br /> Benzene 208 5 200 104 60 142 <br /> Tnchloroethene 210 20 200 105 60 142 <br /> Toluene 214 5 200 107 58 143 <br /> Chlorobenzene 206 20 200 103 57 144 <br /> Ethylbenzene 213 5 200 106 58 147 <br /> m p Xylene 216 5 200 108 57 147 <br /> o-Xyiene 218 5 200 109 58 149 <br /> Surr 1 2 Oichloroethane-d4 179 200 89 70 120 <br /> Surr Toluene-d8 213 200 106 79 124 <br /> Surr 4-Bromofluorobenzene 191 200 95 75 122 <br />