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. Pressure was applied to the vessel with a hand pump and the filtrate directed into the <br /> appropriate containers Each filter was used once and discarded <br /> Sample Preservation and Handling <br /> The following section specifies sample containers, preservation methods, and sample <br /> handling procedures <br /> Sample Containers and Preservation <br /> Sample containers vary with each type of analytical parameter Container types and <br /> materials were selected to be nonreactive with the particular analytical parameter tested <br /> Sample Handling <br /> Sample containers were labeled immediately prior to sample collection Samples were kept <br /> cool with cold packs until received by the laboratory At the time of sampling, each sample <br /> was logged on a chain-of-custody record that accompanied the sample to the laboratory <br /> Samples that required overnight storage prior to shipping to the laboratory were kept cool <br /> i (4°Celsius) in a refrigerator The refrigerator was kept in a warehouse which was locked <br /> when not occupied by an EMCON employee A sample/refrigerator log was kept to <br /> record the date and time that samples were placed into and removed from the refrigerator <br /> Samples were transferred from EMCON to an approved laboratory by courier or taken <br /> directly to the laboratory by the environmental sampler Sample shipments from EMCON <br /> to laboratories performing the selected analyses routinely occurred within 24 hours of <br /> sample collection <br /> Sample Documentation <br /> The following procedures were used during sampling and analysis to provide chain-of- <br /> custody control during sample handling from collection through storage Sample <br /> documentation included the use of the following <br /> Water sample field data sheets to document o Chain-of-custody record sheets for <br /> sampling activities in the field documenting possession and transfer of <br /> samples <br /> ® Labels to identify individual samples <br /> ® Laboratory analysis request sheets for <br /> documenting analyses to be performed <br /> SAC\N\PI0\0F90+DF900020 5AS-95Vw i A-4 Revision 1 8/15/96 <br />