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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> 4991ent. EMCON Service Request S9600801 <br /> Project Teichert-Stockton/20F90-002 004/F ask 001 Date Collected- 5/17/96 <br /> Sample Matrix Water Date Received: 5/21/96 <br /> Date Extracted NA <br /> Date Analyzed- 5/24-28/96 <br /> BTEX and TPH as Gasoline <br /> EPA Methods 5030/8020/Califorrua DHS LUFT Method <br /> TPH as Xylenes, <br /> Analyte Gasoline Benzene Toluene Ethylbenzene Total <br /> Units ug/L(ppb) ug/L(Ppb) ug/L(ppb) ug/L(ppb) ug/L(ppb) <br /> Method Reporting Limit 50 0 5 05 05 05 <br /> Sample(Mame Lab Code <br /> MW-9 59600801-001 ND ND ND ND ND <br /> MW-10 S9600801-002 ND ND ND ND ND <br /> MW-1 1 59600801-003 270* ND ND ND 10 <br /> MW-14 59600801-004 2,500 45 9 24 160 <br /> Method Blank S960524-WBl ND ND ND ND ND <br /> Method Blank S960528-WB1 ND ND ND ND ND <br /> * Sample wntains a higher boiling point hvdrocarbon mixture quantitated as gasoline The <br /> chromatogram does not match the typical gasoline fingerprint <br /> ,ASTXGASl061644 <br /> Page 3 <br />