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Alpha Analytical, Inc. 255 Glendale Ave. • Suite 21 • Sparks,Nevada 89431-5778 {775}355-1044 •(775) 355-0406 FAX e 1-800-283-1153 Work Order: ate: oc Summary Report 43061929 p =03 Method Blank Type MBLK Test Code: EPA Method SW6020 File ID: 06260331001_ICB.DI Batch ID:8065 Analysis Date: 061271200312:07 2003 Sample ID: MB-8065 Units : pg1L Run ID:ICP/MS_030627A Prep Date: 06!27!%RP Analyte Result PQL SpkVal SpkRefVal %REG Lowl-imit Highl-imit RPD Ref Val RPD Qual Lead ND 1 Laboratory Control Spike Type LCS Test Code: EPA Method SW6020 File ID:062603.B1002_LCS.D1 Batch ID:8065 Analysis Date: 06/2712003 12:12 Sample ID: LCS-8065 Units: pg1L Run ID:ICPIMS_030627A Prep Date: 06!2712003 Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Lead 240 1 250 96 85 115 Sample Matrix Spike Type MS Test Code:EPA Method SW6020 File ID: 062603.81007SMPL.D1 Batch ID:8065 Analysis Date: O612712003 12:33 Sample ID: 03061821-05AMS Units : pg1L Run ID:ICPIMS_030627A Prep Date: 0612712003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Lead 247 1 250 18.12 92 70 130 Sample Matrix Spike Duplicate Type MSD Test Code:EPA Method SW6020 File ID: 062603.B%008SMPL.D1 Batch 1D.8065 Analysis Date: 06127/2003 12:37 Sample ID: 03061821-05AMSD Units: pglL Run ID:ICPIMS_030627A Prep Date: 0612012003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Lead 248 1 250 18.12 92 85 115 247.4 0.0872 ents: NA-Not Detected at the Reporting Limit. D-If the spiked value is X25%of the reference value,recovery should not be calculated. �mm S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery fimits due to matrix. B-Analyte detected in the associated Method Blank. Reported in micrograms per liter,per client request.