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Alpha Analytical, Inc. <br /> 255 Glendale Ave. - Suite 21 - Sparks,Nevada 89431-5778 <br /> (775) 355-1044-(775) 355-0406 FAX- 1-800-283-1183 <br /> Date; Work Summary Report Work Order: <br /> 30-Dec-02 02121604 <br /> Method Blank Type:MBLK Test Code: EPA Method SW8260B <br /> File ID:C:kHPCHEM%MSO41DATA1021218k02121807.D Batch ID:MS4W1218A Analysis Date: 1211812002 10.55 <br /> Sample ID: MBLK MS4W1218A Units:pg1L Run 1D:GC/MSD-4-021218A Prep Date, 1211812002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.5 <br /> Di-Isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 0.5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0.5 <br /> 1,2-Dibromoethane(EDB) ND 2 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr: 1,2-Dichloroethane-d4 10.1 10 101 71 130 <br /> Surr:Toluene-d8 9.95 10 100 69 127 <br /> Surr:4-Bromofluorobenzene 10.2 10 102 80 123 <br /> Laboratory Control Spike Type:LCS Test Code:EPA Method SW8260B <br /> File ID:C:IHPCHEMIMS04kDATA1021218102121805.D Batch ID:MS4W1218A Analysis Date: 121181200210:09 <br /> Sample ID: LCS MS4W1218A Units:pg1L Run ID:GCIMSD 4-021218A Prep Date: 12/18/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 10.9 0.5 10 109 80 120 <br /> Toluene 10.7 0.5 10 107 80 120 <br /> � <br /> hylbenzene 11 0.5 10 110 80 120 <br /> p-Xylene 22.2 0.5 20 111 73 129 <br /> Xylene 11.1 0.5 10 111 73 127 <br /> 5urr. 1,2-Dichloroethane-d4 10.4 10 104 71 130 <br /> Sum Toluene-d8 10.2 10 102 69 127 <br /> Surr:4-Bromofluorobenzene 9.9 10 99 80 123 <br /> Sample Matrix Spike Type:MS Test Code:EPA Method SW8260B <br /> File ID: C:IHPCHEMkMSO41DATA1021218102121808.D Batch ID:MS4W7218A Analysis Date: 1211812002 11:26 <br /> Sample ID: 02121604-02AMS Units:pg1L Run ID:GCIMSD_4_021218A Prep Date: 12118/2002 <br /> Analyte Result PQL SpkVal SpkReNal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 48.2 1.3 50 0 96 80 120 <br /> Toluene 46.5 1.3 50 0 93 80 120 <br /> Ethylbenzene 50 1.3 50 1.9 96 80 120 <br /> m,p-Xylene 97.7 1.3 100 2.13 96 73 129 <br /> o-Xylene 48 1.3 50 0 96 73 127 <br /> Surr: 1,2-Dichloroethane-d4 52.7 50 105 71 130 <br /> Surr:Toluene-d8 48 50 96 69 127 <br /> Surr.4-Bromofluorobenzene 49.2 50 98 80 123 <br /> Sample Matrix Spike Duplicate Type:MSD Test Code:EPA Method SW8260B <br /> File ID: C:kHPCHEMkMSO4kDATAk021218k02121809.D Batch ID:MS4W1218A Analysis Date: 12/18/2002 11:49 <br /> Sample ID: 02121604-02AMSD Units :pg1L Run ID:GC/MSD-4-021218A Prep Date: 1211812002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 47.5 1.3 50 0 95 80 120 48.15 1.32 <br /> Toluene 46.3 1.3 50 0 93 80 120 46.46 0.41 <br /> Ethylbenzene 49.4 1.3 50 1.9 95 80 i20 50.04 1.38 <br /> m,p-Xylene 97.9 1.3 100 2.13 96 73 129 97.74 0.167 <br /> o-Xylene 48.3 1.3 50 0 97 73 127 48.04 0.602 <br /> Surr: 1,2-Dichloroethane-d4 51.2 50 102 71 130 <br /> Surr:Toluene-dB 50 50 100 69 127 <br /> rr:4-Bromofluorobenzene 49.2 50 98 80 123 <br />