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alpha analytical, Inc. <br /> 255 Glendale Ave. o Suite 21 • Sparks,Nevada 89431-5778 <br /> (775) 355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> QcSUri1ma Re Wark Order: <br /> *-t..-.02 Q � Ort p 02091146 <br /> Method Blank Type:MBLK Test Code:SW8015 Batch ID:MS12WO912B <br /> File ID-D:IMSDCHEMIMS121DATA1020912102091205.D Analysis Date: 09112/2002 09:42 <br /> Sample ID: MBLK MS12WO912B Units: pg1L Run 10:GC/MSD-12020912A Prep Date: 09/12/2002 <br /> Anaiyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable ND 50 <br /> Surr: 1,2-Dichloroethane-d4 10.8 10 108 71 130 <br /> Surr:Toluene-d8 9.82 10 98 69 127 <br /> Surr:4-Bromofluorobenzene 10.5 10 105 80 123 <br /> Laboratory Control Spike Type:LCS Test Code:SW8015 Batch ID:MS12W091213 <br /> File ID:D:IMSDCHEM1MS121DATA1020912102091203.D Analysis Date: 09/12/2002 09:00 <br /> Sample ID: GLCS MS12WO912B Units:pg1L Run ID:GCIMSD_12_020912A Prep Date: 09/12/2002 <br /> Analyte Result PQL SpkVal SpkRelVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 468 50 400 117 58 136 <br /> Surr: 1,2-Dichloroethane-d4 11.4 10 114 71 130 <br /> Surr.Toluene-d8 9.34 10 93 69 127 <br /> Sum 4-Bromofluorobenzene 10 10 100 80 123 <br /> Sample Matrix Spike Type:MS Test Code:SW8015 Batch ID:MS12WO912B <br /> File ID:D:IMSDCHEM1MS121DATA1020912102091208.D Analysis Date: 09/1212002 10:46 <br /> Sample ID: 02091036-02AGS Units:pg1L Run ID:GCIMSD_12_020912A Prep Date: 09/12/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowL[mit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 2240 250 2000 0 112 58 136 <br /> Surr: 1,2-Dichloroethane-d4 51 50 102 71 130 <br /> Surr:Toluene-d8 47.8 50 96 69 127 <br /> ddiurr:4-Bromofluorobenzene 50.6 50 101 80 123 <br /> ample Matrix Spike Duplicate Type:MSD Test Code:SW8015 Batch ID:MS12W09125 <br /> File ID: D:IMSDCHEMIMS121DATA1020912102091209.D Analysis Date: 09112/2002 11:07 <br /> Sample ID: 02091036-02AGSD Units:pglL Run ID:GC/MSD-12_020912A Prep Date: 09/12/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qua[ <br /> TPH Purgeable 2240 250 2000 0 112 58 136 2238 0.183 <br /> Surr: 1,2-Dichloroethane-d4 48.9 50 98 71 130 <br /> Surr:Toluene-d8 48.4 50 97 69 127 <br /> Surr:4-Bromofluorobenzene 49.7 50 99 80 123 <br /> Comments: ND-Not Detected at the Reporting Limit. D-ff the spiked value is<25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B -Analyte detected in the associated Method Blank. <br /> Reported in micrograms per liter,per client request. <br />