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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: EMCON Service Request: S9901001 <br /> Project: Tcichert&Sons-Stockton/20F90-002.007 Date Collected: 3/23/99 <br /> Sample Matrix: Soil Date Received: 3/25/99 <br /> Fuel Oxygenates <br /> Sample Name: SP-5AB Units: ug/Kg{ppb} <br /> Lab Code: S9901001-029 Basis: Wet <br /> Test Notes: <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> Cert-Butyl Alcohol NONE 8260 500 1 4/2199 4/3/99 ND <br /> Methyl Cert-Butyl Ether NONE 8260 5 1 4/2199 4/3/99 ND <br /> Diisopropyl Ether NONE 8260 50 1 4/2/99 4/3/99 ND <br /> Ethyl Cert-Butyl Ether NONE 8260 50 1 4/2/99 4/3/99 ND <br /> tert-Amyl Methyl Ether NONE 8260 50 1 4/2/99 4/3/99 ND <br /> . arwwcnrP <br /> Paae 7 <br />