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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> client: EMCON Service Request: 59901001 <br /> Project: Teichert& Son s-S tockton/20F90-002.007 Date Collected: 3123/99 <br /> Sample Matrix: Soil Date Received. 3/25/99 <br /> Fuel Oxygenates <br /> Sample Name: SP-5A/13 Units: ug/Kg(ppb) <br /> Lab Code: 59901001-029 Basis: Wet <br /> Test Notes: <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRI, Factor Extracted Analyzed Result Notes <br /> tert•Butyl Alcohol NONE 8260 500 1 4/2/99 413/99 ND <br /> Methyl tert-Butyl Ether NONE 8260 5 1 4/2/99 4/3/99 ND <br /> Diisopropyl Ether NONE 8260 50 1 4/2/99 4/3/99 ND <br /> Ethyl tert-Butyl Ether NONE 8260 50 l 4/2199 4/3/99 ND <br /> Cert-Amyl Methyl Ether NONE 8260 50 1 4/2/99 4/3/99 ND <br />