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COLUMBIA ANALYTICAL SERVICES, INC. <br /> Analytical Report <br /> Tient: EMCON Service Request: 59901001 <br /> Project: Teichert&Sons-Stockton/20F90-002.007 Date Collected: 3/24/99 <br /> Sample Matrix: Soil Date Received: 3/25/99 <br /> Fuel Oxygenates <br /> Sample Name: SP-10A/B Units: ug/Kg(ppb) <br /> Lab Code: S9901001-034 <br /> Test Notes. Basis: Wet <br /> Prep Analysis Dilution Date /late Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> tert-Butyl Alcohol NONE 8260 500 l 4/2/99 4/5/99 ND <br /> Methyl Cert-Butyl Ether NONE 8260 5 1 4/2/99 4/5/99 20 <br /> Diisopropyl Ether NONE 8260 50 1 4/2/99 4/5/99 ND <br /> Ethyl tert-Butyl Ether NONE 8260 50 1 4/2/99 4/5/99 ND <br /> tert-Amyl Methyl Ether NONE 8260 50 1 4/2199 4/5/99 ND <br /> i <br />