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, L <br /> Alpha Analytical, Inc. <br /> 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX • 1-800-283-1183 <br /> Date <br /> 30 Dec 03 QC Summary Report Work <br /> der <br /> 42 <br /> Method Blank Type MBLK Test Code EPA Method SW82608 <br /> File ID C 1HPCHEMIMS071DATA1031219103121904 D Batch ID MS07W1219A Analysis Date 12/19/2003 09 05 <br /> Sample ID MBLK MS07W1219A Units pg/L Run ID GC/MSD 7 031219A Prep Date 12/19/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit f ighLimd RPDRefVal %RPD(lamit) Qual <br /> Tertiary Butyl Alcohol (TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 05 <br /> Di-isopropyl Ether(D1PE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 0 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 05 <br /> 1,2-Dibromoethane (EDB) ND 2 <br /> Ethylbenzene ND 05 <br /> m,P-XWene ND 05 <br /> o-Xylene ND 0 5 <br /> Surr 1,2-Dichloroethane-d4 9 41 10 94 72 126 <br /> Surr Toluene-d8 104 10 104 71 128 <br /> Surr 4-Bromofluorobenzene 9 39 10 94 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SWa2608 <br /> File ID C 1HPCHEM\MS071DATA1031219103121903 D Batch ID MS07W1219A Analysis Date 12/19/2003 08 42 <br /> Sample ID LCS MS07W1219A Units pg/L Run ID GC/MSD-7-031219A Prep Date 12/19/2003 <br /> Analyte Result PQL SpkVal SpkRefVa1 %REC LowiLimit HighUmit RPDRefVal %RPD(Limrt) Qual <br /> 1 2-Dichloroethane9 53 1 10 95 68 126 <br /> enzene 107 05 10 107 83 119 <br /> oluene 115 0 5 10 115 80 120 <br /> 1,2 Dibromoethane(EDB) 10 2 10 100 68 131 <br /> Ethylbenzene 119 0 5 10 119 80 120 <br /> m,p-Xylene 249 05 20 125 77 125 <br /> o-Xylene 117 05 10 117 77 124 <br /> Surr 1,2-Dichloroethane-d4 953 10 95 72 126 <br /> Surr Toluene-d8 107 10 107 71 128 <br /> Surr 4-Bromofluorobenzene 958 10 96 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID C 1HPCHEM1MS071DATA1031219103121910 D Batch ID MS07W1219A Analysis Date 12/19/2003 11 19 <br /> Sample ID 03121807-02AMS Units pg/L Run fD GC/MSD-7-031219A Prep Date 12/19/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmd HighLimit RPDRefVal %RPD(Limit) Qual <br /> 1,2-Dichloroethane 48 25 50 0 96 41 151 <br /> Benzene 548 13 50 0 110 59 145 <br /> Toluene 58 13 50 0 116 39 161 <br /> 1,2-Dibromoethane(EDB) 522 10 50 0 104 51 146 <br /> Ethylbenzene 58 9 1 3 50 0 118 57 145 <br /> m p-Xylene 125 1 3 100 0 125 37 163 <br /> o-Xylene 58 6 1 3 50 0 117 47 156 <br /> Surr 1 2-Dichloroethane-d4 473 50 95 72 126 <br /> Surr Toluene-d8 533 50 107 71 128 <br /> Surr 4-Bromofluorobenzene 476 50 95 76 121 <br /> Sample Matnx Spike Duplicate Type MSD Test Code EPA Method SW826013 <br /> File ID C1HPCHEMIMS07\DATA1031219103121911 D Batch ID MS07W1219A Analysis Date 12/19/2003 11 41 <br /> Sample ID 03121807-02AMSD Units pg/L Run ID GC/MSD-7-031219A Prep Date 12/19/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighUmit RPDReNal %RPD(Limit) Qua] <br /> 1,2-Dichloroethane 487 25 50 0 97 41 151 4803 1 4(24) <br /> Benzene 541 1 3 50 0 108 59 145 5482 1 3(22) <br /> -ene 566 13 50 0 113 39 161 58 02 2 5(22) <br /> Dibromoethane(EDB) 52 9 10 50 0 106 51 146 5216 1 3(24) <br /> thylbenzene 678 1 3 50 0 116 57 145 58 89 1 9(22) <br /> m,p-Xy]ene 122 1 3 100 0 122 37 163 1253 2 6(23) <br /> o-Xylene 569 1 3 50 0 114 47 156 58 6 2 9(50) <br /> Surr 1 2-Dichloroethane-d4 48 7 50 97 72 126 <br /> Surr Toluene-d8 526 50 105 71 128 <br /> Surr 4-Brom0fluorobenzene 474 50 95 76 121 <br />