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American Envlf-onmental Network <br /> WORK ORDER 9710281 QUALITY CONTROL REPORT PAGE QR-3 <br /> ANALYSIS Gasoline Oxygenates <br /> MATRIX Water <br /> MATRIX SPIKE SAMPLES <br /> SAMPLE TYPE Spike Sample/Matrix LAB ID MS10281 03A INSTR RUN GCMS13\971027000000/32/31 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13W102997 <br /> UNITS ug/L ANALYZED 10/29/97 DILUTION 1 00 <br /> METHOD EPA 8260 <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCE d4 (surr) 130 114 100 100 130 70 130 <br /> Toluene d8 (surr) 102 105 100 100 102 70 130 <br /> Bromofluorobenzene (surr) 96 2 95 6 100 100 96 2 70 130 <br /> Methy t butyl ether (MTBE) 136 ND 5 100 136 32 158 <br /> Ethyl t butyl ether (ETBE) 144 ND 5 100 144 32 158 <br /> t Amylmethyl ether (TAME) 118 ND 5 100 118 32 158 <br /> MATRIX SPIKE DUPLICATES <br /> SAMPLE TYPE Spiked Sample Duplicate LAB ID MR10281 03A INSTR RUN GCMS13\971027000000/34/32 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13W102997 <br /> UNITS ug/L ANALYZED 10/30/97 DILUTION 1 00 <br /> METHOD EPA 8260 <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCE d4 (surr) 119 130 100 100 119 70 130 <br /> Toluene d8 (surr) 106 102 100 100 106 70 130 <br /> Bromofluorobenzene (surr) 95 4 96 2 100 100 95 4 70 130 <br /> Methy t butyl ether (MTBE) 112 136 5 19 4 25 <br /> Ethyl t butyl ether (ETBE) 121 144 5 17 4 25 <br /> t Amylmethyl ether (TAME) 99 6 118 5 16 9 25 <br /> - - -- - - - - - - - - - - - - - -- - - <br /> SAMPLE SURROGATES <br /> SAMPLE TYPE Sample-Client LAB ID 9710281 01A INSTR RUN GCMS13\971027000000/29/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13W102997 <br /> UNITS ug/L ANALYZED 10/29/97 DILUTION 1 00 <br /> METHOD EPA 8260 <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (�) <br /> 1 2 DCE d4 (surr) 130 100 100 130 70 130 <br /> Toluene d8 (surr) 105 100 100 105 70 130 <br /> Bromofluorobenzene (surr) 99 2 100 100 99 2 70 130 <br /> SAMPLE TYPE Sample Client LAB ID 9710281 02A INSTR RUN GCMS13\971027000000/30/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13W102997 <br /> UNITS ug/L ANALYZED 10/29/97 DILUTION 1 00 <br /> METHOD EPA 8260 <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCE d4 (surr) 109 100 100 109 70 130 <br /> Toluene d8 (surr) 113 100 100 113 70 130 <br /> Bromofluorobenzene (surr) 99 0 100 100 99 0 70 130 <br /> SAMPLE TYPE Sample Client LAB ID 9710281 03A INSTR RUN GCMS13\971027000000/31/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13W102997 <br /> UNITS ug/L ANALYZED 10/29/97 DILUTION 1 00 <br /> METHOD EPA 8260 <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br />. ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> , 1 2 DCE d4 (surr) 114 100 100 114 70 130 <br /> Toluene d8 (surr) 105 100 100 105 70 130 <br /> Bromofluorobenzene (surr) 95 6 100 100 95 6 70 130 <br /> End of Quality Control Report <br />