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1b inSuperior Analytical Laboratory ,SECOR Project KING ISLAND Attn TERRY PLUNKETT Reported on February 2, 1996 Total Petroleum Hydrocarbons as Diesel ' by EPA SW-846 Method b015M Diesel Range quantitated as all compounds from C10-C25 QC Batch ## QC Sample ID TypeRef Matrix Extract Analyzed CA292 29-02 Laboratory Spike LS Soil 01/29/96 01/29/96 CA292 29-03 Laboratory Spike Duplicate LSD Soil 01/29/96 01/29/96 CA292 29-04 B1-11 MS 20842-03 Soil 01/29/96 01/30/96 CA292 29-05 B1-11 MSD 20842-03 Soil 01/29/96 01/30/96 CA311 21-01 Method Blank MB Soil 01/31/96 01/31/96 CA311 21-02 Laboratory Spike LS Soil 01/31/96 01/31/96 CA311 21-03 Laboratory Spike Duplicate LSD Soil 01/31/96 01/31/96 CA311 21-04 SB-7,3 5 MS 20843-55 Soil 01/31/96 01/31/96 CA311 21-05 SB-7, 3 5 MSD 20843-55 Soil 01/731/96 01/31/96 CA311 42-01 Method Blank MB Water 01/31/96 01/31/96 CA311 42-02 Laboratory Spike LS Water 01/31/96 01/31/96 CA311 42-03 Laboratory Spike Duplicate LSD Water 01/31/96 01/31/96 CA261 21-01 Method Blank MB Water 01/26/96 01/26/96 CA261.21-02 Laboratory Spike LS Water 01/26/96 01/26/96 CA261 21-03 Laboratory Spike Duplicate LSD Water 01/26/96 01/26/96 CA271 29-01 Method Blank MB Soil 01/27/96 01/27/96 CA271 29-02 Laboratory Spike LS Soil 01/27/96 01/27/96 CA271 29-03 Laboratory Spike Duplicate LSD Soil 01/27/96 01/27/96 CA271 29-04 SB-2, 3 5 MS 20843-22 Soil 01/27/96 01/27/96 CA271 29-05 SB-2, 3 5 MSD 20843-22 Soil 01/27/96 01/27/96 CA301 42-01 Method Blank MB Water 01/30/96 01/30/96 CA301 42-02 Laboratory Spike LS Water 01/30/96 01/30/96 CA301 42-03 Laboratory Spike Duplicate LSD Water 01/30/96 01/30/96 Page 2 of 16