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n <br /> - s Superior <br /> h <br /> S <br /> Analytical Laboratory <br />' Total Petroleum Hydrocarbons as Diesel <br /> by EPA SW-846 Method 8015M <br /> Diesel Range quantitated as all compounds from C10-C25 <br /> Quality Assurance and Control Data <br /> j <br />' Laboratory Number 20843 <br /> Compound Sample SPK Level SPK Result Recovery Limits RPD <br /> conc $ o <br /> For Soil Matrix (mg/Kg) <br /> CA271 29 02 / 03 - Laboratory Control Spikes <br /> Diesel 33 34/28 103/85 50-150 19 <br />�> Surrogate Recoveries (t) « <br /> Tetracosane 103/86 50-150 <br />' For Water Matrix (ug/L) <br /> CA301 42 02 / 03 - Laboratory Control Spikes <br /> Piesel <br /> 1000 1020/980 102/98 50-150 --w4 <br />�> Surrogate Recoveries (t) « - y <br /> Tetracosane 74/77 50-150 <br /> For Soil Matrix (mg/Kg) <br /> CA292 29 04 / 05 - Sample Spiked 20842 - 03 <br /> Diesel ND 33 33 7/32 4 102/98 - 50-150 4 <br /> >> Surrogate Recoveries (t) « <br /> Tetracosane 97/91 50-150 <br /> For Soil Matrix (mg/Kg) <br /> CA311 21 04 / 05 - Sample Spiked 20843 - 55 <br /> Diesel ND 33 29 4/31 2 89/95 50-150 7 <br />�•> Surrogate Recoveries ¢< <br /> Tetracosane 93/95 50-150 <br /> 6 <br /> Page 15 of 16 <br />