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N t w Ames ican E w w7mental Network WORK ORDER 9803262 QUALITY CONTROL REPORT PAGE QR-6 ANALYSIS Gasoline Oxygenates MATRIX Water SAMPLE SURROGATES SAMPLE TYPE Sample Client LAB ID 9803262 04E INSTR RUN GCMS12\980401000000/10/ INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12WO40198 UNITS ug/L ANALYZED 04/02/98 DILUTION 1 00 METHOD REF REPORTING SPIKE RECOVERY REC. LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (%) LIMIT (X) 1 2 DCE d4 (surr) 117 100 100 117 70 135 Toluene d8 (surr) 111 100 100 111 70 130 Bromofluorobenzene (surr) 88 1 100 100 88 1 70 130 SAMPLE TYPE Sample Client LAB ID 9803262 05F INSTR RUN GCMS12\980401000000/11/ INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12WO40198 UNITS ug/L ANALYZED 04/02/98 DILUTION 100000 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE __ RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1 2 DCE d4 (surr) 98 5 10000000 100 98 5 70 135 Toluene d8 (surr) 104 10000000 100 104 70 130 Bromofluorobenzene (surr) 93 8 10000000 100 93 8 70 130 SAMPLE TYPE Sample Client LAB ID 9803262 06F INSTR RUN GCMS12\980401000000/13/ INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12WO40198 UNITS ug/L ANALYZED 04/02/98 DILUTION 1 00 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1 2 DCE d4 (surr) 98 0 100 100 98 0 70 135 Toluene d8 (surr) 110 100 100 110 70 130 Bromofluorobenzene (surr) 88 3 100 100 88 3 70 130 SAMPLE TYPE Sample Client LAB iD 9803262 07F INSTR RUN GCMS12\980401000000114/ INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12WO40198 UNITS ug/L ANALYZED 04/02/98 DILUTION 1 00 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1 2 DCE d4 (surr) 105 100 100 105 70 135 Toluene d8 (surr) 106 100 100 106 70 130 Bromofluorobenzene (surr) 90 0 100 100 90 0 70 130