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Sequoia 680 Chesapeake Dnve Redwood City,CA 94063 (650) 364-9600 FAX(650)364 9233 <br /> 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988-9600 FAX(510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento, CA 95834 (916) 911-9600 FAX(916) 921 0100 <br /> Blaine Tech Services Client Prol ID Shell Stockton/971009-G1 Sampled 10/09/97 <br /> 1680 Rogers Avenue Sample Descript MW-4 Received 10/10/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 10/18/97 <br /> Attention Fran Thie Lab Number 9710591-06 Reported 1OJ23197 <br /> C Batch Number MS101797MTBEI=2A - <br /> istrument ID F2 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detect:on Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Metyl t-Butyl Ether (MTBE) 20 N D <br /> Di-Isopropyl Ether (DIPE) 20 N D <br /> Ethyl t-Butyl Ether (ETRE) 20 N D <br /> t-Amyl Methyl Ether(TAME) 20 N D <br /> Surrogates Control Limits% % Recovery <br /> 1,2-Dichloroethane-d4 76 114 92 <br /> iaiytes reported as N D were not present above the stated limit of detection <br />)E0001A AN L 1CAL - ELAP #1210 <br /> e ner <br /> roject Manager Page 16 <br /> 94 <br />