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Sequoia 680 Chesapeake Dnve Redwood City,CA 94063 (650) 364-9600 FAX(650)364-9233 <br /> 404 N Wtget Lane Walnut Creek,CA 94598 (510) 988-9600 FAX (510) 988-9673 <br /> Analytical 819 Sinker Avenue,Suite 8 Sacramento,CA 95834 (916) 921-9600 FAX (916)921-0100 <br /> • <br /> Blaine Tech Services Client Prol ID Shell Stockton/971009-G1 Sampled 10/09/97 <br /> 1680 Rogers Avenue Sample Descript MW-4 Received 10/10/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method 8015Mod/8020 Analyzed 10/20/97 <br /> Attention Fran Thie Lab Number 9710591-06 Reported 10123197 <br /> DC Batch Number GC102097BTEX02A <br /> nstrument ID GCHP02 <br /> Total Purgealble Petroleum Hydrocarbons (TPPH) with ETEX and MTBE <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> TPPH as Gas 50 N D <br /> Methyl t-Butyl Ether 25 N D <br /> Benzene 050 N D <br /> Toluene 050 N D <br /> Ethyl Benzene 050 N D <br /> Xylenes (Total) 0 50 N D <br /> Chromatogram Pattern <br /> Surrogates Control Limits % % Recovery <br /> Trifluorotoluene 70 130 98 <br /> 0 <br />%nalytes reported as N D were not present above the stated limit of detection <br /> 3EQU A ALVTICAL - ELAP #1210 <br /> Aenner <br /> rolect Manager Page 18 <br />