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i <br /> I 10 Second Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> grip//www mccampbell corn E-mail main@mccampbell com <br /> IAdvanced GeoEnvironmental Client Protect ID Den's Auto Date Sampled 09108-09/11/97 <br /> Date Received 09/13/97 <br />' 1803 West March Lane, Ste A <br /> Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/15/97 <br /> Client P O Date Analyzed 09/15-09116/97 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 80770 <br /> Client ID 134-43 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<20 trans 1,3-Dichloropiopene ND<20 <br /> Benzene 140 Ethylene dibromide'u ND<20 <br /> Bromobenzene ND<20 Ethylbenzene 120 <br /> Bromochloromethane ND<20 Hexachlorobutadiene ND<20 <br />' Bromodichloromethane ND<20 lodomethane ND<20 <br /> Bromoform ND<20 Isopropylbenzene 45 <br /> Bromomethane ND<20 p-Isopropyl toluene ND<20 <br /> n-Butyl benzene 44 Methyl butyl acetone"' ND<20 <br />' sec-Butyl benzene ND<20 Methylene Chloride" ND<20 <br /> tert Butyl benzene 22 Methyl ethyl ketone"' ND<20 <br /> Carbon Disulfide ND<20 Methyl isobutyl ketone' ' ND<20 <br /> Carbon Tetrachloride ND<20 Methyl tert-Butyl Ether(MTBE) --- <br />� . Chlorobenzene ND<20 Napthalene ND<25 <br /> Chloroethane ND<20 n-Propyl benzene ND<20 <br /> 2-Chloroethyl Vinyl Etbe ` ND<20 St3rene" ND<20 <br /> Chloroform ND<20 a 1 1 2 Tetrachloroethane ND<20 <br />' Chloromethane ND<20 1 1 2 2 Tetrachloroethane ND<20 <br /> 2-Chlorotoluene ND<20 Tetrachloroethene ND<20 <br /> 4-Chlorotoluene ND<20 Toluene""' ND<20 <br /> Dibromochloromethane ND<20 1,2 3-TrichlOTobenzene ND<20 <br /> 1,2-Dibromo 3-chloropropane ND<20 1 24-Trichlorobenzene ND<20 <br /> Dibromomethane ND<20 1,1,1-Trichloroethane ND<20 <br /> 1,2-Dichlorobenzene ND<20 1,1 2-Trichloroethane ND<20 <br /> 1,3 Dichlorobenzene ND<20 Trichloroethene ND<20 <br /> 1,4-Dichlorobenzene ND<20 Trichlorofluoromethane ND<20 <br /> Dichlorodifluoromethane ND<20 1 2 3-Ti ichloropropane ND<20 <br /> I,1-Dichloroethane ND<20 1,24 Tiimethylbenzene ND<20 <br /> 1 2-Dichloroethane ND<20 1 3 5-Trimetbylbenzene 56 <br />' 1,1-Dich1oroethene ND<20 Vinyl Acetate"" ND<20 <br /> cis-1,2-Dichloroethane ND<20 Vinyl Chloride"' ND<20 <br /> trans-l,2-Dichloroethene ND<20 X)lenes,total `°' ND<20 <br /> 1,2-Dichloropropane ND<20 Comments J <br />' 1,3-Dichloropropane ND<20 Surrogate Recoveries(%} <br /> 2,2-Dichloropropane ND<20 Dibromolluoromethane 85 <br /> 1,1-Dichloropropene ND<20 Toluene-d8 99 <br />' cis-1,3-Dicbloropropene ND<20 4 Bromot7v01-obenzene 91 <br /> water and vapor samples are reported m uglL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP!SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,%apor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2 hexanone (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 ��� Edward Hamilton, Lab Director <br />