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1 <br /> 110 Second Avenue South,#D7,Pacheco,CA 94553 <br />' MCCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Den's Auto Date Sampled 09/08-09/11/97 <br />' 1803 West March Lane, Ste A <br /> Date Received 09/13/97 <br /> Stockton,CA 95207 Client Contact Bill Little Date Extracted 09/15/97 <br />' Client P O Date Analyzed 09/15-09/16/97 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab 1D 80769 <br /> Client 1D 134-57 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<100 trans-1,3 Dichloropropene ND<100 <br /> Benzene 910 Ethylene dibromide' ' ND<100 <br /> Bromobenzene ND<100 Ethylbenzene 1700 <br /> Bromochloromethane ND<100 1-lexachlorobutadiene ND<100 <br />' Bromodichloromethane ND<100 lodomethane ND<100 <br /> Bromoform ND<100 lsopropylbenzene 340 <br /> Bromomethane ND<100 p-Isopropyl toluene ND<100 <br /> n-Butyl benzene 470 Methyl butyl ketone"' ND<100 <br />' sec-Butyl benzene 130 Methylene Chloride' ND<100 <br /> tert-Butyl benzene 200 Methyl ethyl acetone`s' ND<100 <br /> Carbon Disulfide ND<100 Methyl 3sobutyl ketone' ' ND<100 <br /> Carbon Tetrachloride ND<100 Methyl tert-Butyl Ether(MTBE) --- <br />' Chlorobenzene ND<100 Napthalene 1300 <br /> Chloroethane ND<100 n-Propyl benzene ND<100 <br /> 2-Chloroethyl Vinyl Ether" ND<100 Styrene'' ND<100 <br /> Chloroform ND<l 00 1,1,1,2-Tetr ach I oroethane ND<100 <br /> Chloromethane ND<100 1,1,2,2-Tetrachloroethane ND<100 <br /> 2-Chlorotoluene ND<100 Tetrachloroethene 150 <br /> 4-Chlorotoluene ND<100 Toluene""' ND<100 <br /> Dibromochlommethane ND<100 1,2,3-Trichlorobenzene ND<100 <br />' 1,2-Dibromo-3-chloropropane ND<100 1,2,4-Triclilorobenzene ND<100 <br /> Dibromomethane ND<100 1,1,1-Trichloroethane ND<100 <br /> 1,2-Dichlorobenzene ND<100 1 32 Trichloroethane ND<100 <br /> 1,3-Dichlorobenzene ND<100 Trichloroethene ND<100 <br /> 14-Dichlorobenzene ND<100 Tnchiorofluoromethane ND<100 <br /> Dichlorodifluoromethane ND<100 12,3-Trichloropmpane ND<100 <br /> 1,1-Dichloroethane ND<100 1,2 4-Trimethylbenzene ND<100 <br /> 1 2-Dichloroethane ND<100 1,3,5 Tnmethylbenzene ND<100 <br /> 1,1-Dichloroethene ND<100 Vinyl Acetate"" 770 <br /> cis-1,2-Dichloroethene ND<100 Vinyl Chloride'°' ND<100 <br /> trans-l,2-Dichi oroethene ND<100 X)lenes,total " 690 <br /> 1,2-Dichloropropane ND<100 Comments <br /> 1,3-Dichloropropane ND<100 Surrogate Reco%eries(%) <br /> 2,2-Dichloropropane ND<100 Dibromofluoromethane 81 <br /> 1,1-Dichloropropene ND<100 Toluene-d8 99 <br />' cis-1,3-Dichloropropene ND<100 4-Bromotluorobenzene 92 <br /> eater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and 211 TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L I apor samples 0 5 u,-/L solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content (k) ethenylbenzene (i) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chaoroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 �,� Edward Hamilton,Lab Director <br />