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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> httt]//www mccam)bell com E-mall main@mccampbell corn <br /> • <br /> 1 Advanced GeoEnvironmental Client Project ID Den's Auto Date Sampled 09108-09/11/97 <br /> 1803 West March Lane, Ste A Date Received 09/13/97 <br />' Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/15/97 <br /> Client P O Date Analyzed 09/15-09116/97 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 80778 <br /> Client ID B6-65 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br />' Acetone' ND trans-l3-Dichloropropene ND <br /> Benzene ND Ethylene dibiomide` ' ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br />' Brotnodichloromethane ND lodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> BTOmomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br />' sec-Butyl benzene ND Methylene Chloride" ND <br /> teri-Butyl benzene ND Methyl ethyl ketone`' ND <br /> Carbon Disulfide ND<10 Methyl isobutyl ketone' ' ND <br /> . Carbon Tetrachloride ND Methyl ten-Butyl Ether(MTBE) <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether"I ND Styrene" ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Cbloromethane ND 3,1,2,2 Tetrachloioethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene""' ND <br /> Dibromochloromethane ND 12,3-"ITnchlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloioethane ND <br /> l2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4 Dichlorobenzene ND Trichlorolluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tiichloropropane ND <br /> ],1-Diehl oroethane ND 1,2,4-Tri methylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Tri methyl benzene ND <br /> 1,1-Dichloroetbene ND Vinyl Acetate1°' ND <br /> ci s-1,2-Di chloroethene ND Vinyl Chloride'°' ND <br /> trans-l,2-Diehl oroethene ND Xylenes,total ND <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Recoieries(%) <br /> E-DicM <br /> pane ND Dibromotluoromethane 98 <br /> -Dicpene ND Toluene-d8 107 <br /> cis-1,3 propene ND 4-Bromofluorobenzene 92 <br /> Water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit NIA means analyte not apphcable to this analysis <br /> (b) 2-proponone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hcaanone, (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene (o}dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />