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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> 24 ht Ilwww mccam bell com E-mail main@mccampbell com <br /> • <br /> Advanced GeoEnvironmental Client Project ID Den's Auto Date Sampled 09/24/97 <br /> 1803 West March Lane, Ste A Date Received 09/25/97 <br /> Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/30/97 <br /> Client P O Date Analyzed 09/30/97 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID81174 <br /> Client ID M W 1-B/9-24-97 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> E Acetone i ND<12 5 trans-1,3-Dichloropropene ND<12 5 <br /> Benzene 270 Ethylene dibromide' ' ND<12 5 <br /> Bromobenzene ND<12 5 Ethvlbenzene 230 <br /> Bromochloromethane ND<12 5 1-fexachlorobutadiene ND<12 5 <br /> Bromodichloromethane ND<12 5 lodomethane ND<12 5 <br /> Bromoform ND-e12 5 Isopropylbenzene 41 <br /> Bromomethane ND<12 5 p-isopropyl toluene ND<12 5 <br /> n-Butyl benzene 18 Methyl butyl ketone"' ND<12 5 <br /> sec-Butyl benzene ND<12 5 Methylene Chloi ide" ND<12 5 <br /> tett Butyl benzene ND<12 5 Methyl ethyl ketone"' iND<12 5 <br /> Carbon Disulfide ND<12 5 Methyl isobutyl ketone' ' ND<12 5 <br />�. Carbon Tetrachloride ND<12 5 Methyl tert Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<12 5 Napthalene 110 <br /> Chloroethane ND<12 5 n-Propyl benzene 60 <br /> 2-Chloroethyl Vinyl Ether` ND<12 5 Styrene" ND<12 5 <br /> Chloroform ND<12 5 1 1 1 2-Tetiacl-iloroethane _ ND<12 5 <br /> Chloromethane ND<12 5 1 1 2,2-Tetiachloroethane ND<12 5 <br /> 2-Chlorotoluene ND<12 5 Tetrachloroethene ND<26 <br /> 4-Chlorotoluene NL><125 Toluene""' 24 <br /> Dibromochloromethane ND<12 5 1,2,3-Tnchlorobenzene ND<12 5 <br /> 1,2-Dibromo-3-chloropropane ND<12 5 1,2 4-Tnchlorobenzene ND<12 5 <br /> DibrOmomethane ND<12 5 1 1 1-Trichloioethane ND<12 5 <br /> 1,2-Dichlorobenzene ND<12 5 1 1 2 Trichloroethane ND<12 5 <br /> 1,3-Dichlorobenzene ND<12 5 Tnehloroethene ND<12 5 <br /> 1,4-Dichlorobenzene ND<12 5 Tnchlorolluoiomethane ND<12 5 <br /> Dichlorodifluoromethane ND<12 5 1 2 3 Trichloropropane ND<12 5 <br /> 1 i-Dichloroethane ND<12 5 1,2 4-Trimethylbenzene 77 <br />' 1,2-Dichloroethane 15 1 3,5-Trimethylbenzene 20 <br /> 1,1 Dichloroethene ND<12 5 Vinyl Acetate"" 26 <br /> cis-1,2-Diehl oroethene ND<12 5 Vmy!Chloride'"' NIX12 5 <br /> trans-1,2-Dichloroethene NLK12 5 Venes,total 'i 140 <br /> 1,2-Dichloropropane ND<12 5 Comments <br /> 1 3-Dichloropropane ND<12 5 Surrogate Recokeries(%} <br /> 2,2-Dichloropropane ND<12 5 Dibromofluoromethane 91 <br /> 1,1-Dichloropropene ND<12 5 Toluene d8 99 <br />' cis-1,3-Dichloropropene ND<12 5 1 4-Bromolluorobenzene 88 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/tripe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L .apor samples 0 5 ug/L solid and sludge samples 5 ug/kg wipes 0 2ug/wipe <br />' ND means not detected above the epomng limit,N/A means analyte not applicable to ibis analyses <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethaxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />