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110 Second Avenue South,#D7, Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> h //www mccam bell com E-mail main@mecampbell corn <br /> Advanced GeoEnvironmental Client Project ID Den's Auto Date Sampled 09/24/97 <br /> 1803 West March Lane, Ste A Date Received 09/25/97 <br /> Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/30/97 <br /> Client P 0 Date Analyzed 09/30/97 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br />' Lab ID 81 176 <br /> Client ID M W2-B/9-24-97 <br /> Matrix W <br /> Compound Concentration* Compound Concentration'" <br /> Acetone` ND<30 trans-] 3-Dichloiopropene ND<30 <br /> Benzene 110 Ethylene dibromide' ' ND<30 <br /> Bromobenzene NTX30 Ethylbenzene 190 <br /> Bromochloromethane ND<30 Hexachlorobutadiene ND<30 <br />' Bromodichloromethane ND<30 lodomethane ND<30 <br /> Bromoform ND<30 Isopropylbenzene 32 <br /> Bromomethane ND<30 p Isopropyl toluene ND<30 <br /> n-Butyl benzene 61 Methyl butyl ketone"' ND<30 <br /> sec-Butyl benzene ND<30 Methylene Chloi ide, ND<30 <br /> tert Butyl benzene 42 Methyl ethyl ketone'K' ND<30 <br /> Carbon Disulfide ND<30 Methyl isobutyl ketone' ' ND<30 <br /> Carbon Tetrachloride ND<30 Methyl Cert-Butyl Ether(MTBE) --- <br />�. Chlorobenzene ND<30 Napthalene 270 <br /> Chloroethane ND<30 n-Propyl benzene 65 <br /> 2-Chioroethyl Vinyl Ether` ND<30 Styrene" ND<30 <br /> Chloroform ND<30 1 1 1,2 Tetrachloroethane ND<30 <br /> Chloromethane ND<30 1,1,2,2 Teti achloioethane ND<30 <br /> 2-Chlorotoluene ND<30 Tetrachlaroethene ND<30 <br /> 4-Chlorotoluene ND<30 Toluene""' NIX30 <br /> Dibromochloromethane ND<30 1 2 3-Trichlorobenzene ND<30 <br /> 1,2-Dibromo-3-chloropropane ND<30 1 2,4-Trichlorobenzene ND<30 <br /> Dibromomethane N13<30 1 1 I Trichloroethane ND<30 <br /> 1,2-Dichlorobenzene ND<30 1 1 2 Trichloroethane ND<30 <br /> 1,3-Dichlorobenzene ND<30 Trichloroethene ND<30 <br /> 1,4-Dichlorobenzene ND<30 Tnehloroi]uoromethane ND<30 <br /> Dichlorodifluoromethane ND<30 1,2 3 Trichloroproparie ND<30 <br /> 1,1-Dichloroethane ND<30 1 2 4-Tnmethylbenzene 820 <br /> 1,2-Dichloroethane ND<30 1 3 Trimethylbenzene 230 <br /> 1 I-Dichloroethene ND<30 Vinyl Acetate"" ND<30 <br /> cis-1,2-Dichloroethene ND<30 VmyI Chloride'" ND<30 <br /> trans-1,2-Dichloroethene ND<30 Xylenes total "" 1500 <br />' 1,2-Dichloroprop3ne ND<30 Comments <br /> 1,3-Dichloropropane ND<30 Surrogate Recorenes(A) <br /> 2,2-Dichloropropane ND<30 Dibromofluoromethane 97 <br /> l,l-Dichloropropene ND<30 Toluene-d8 97 <br /> cis-1,3-Dichloropropene ND<30 4-Bromotluorobenzene 85 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg »ipes in ug/u ipe and ala TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,.3POT samples 0 5 ug/L solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2 hexanone (e) dichloromethane, (i) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropvlacetone (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chlomethene,{o)dirnethylbenzenes . / <br /> DHS Certification No 1644 /h' Edward Hamilton, Lab Director <br />