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k r r • • <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mE22mpbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnviromnental Client Project M:N.El-Dorado at Linds ,Date Sampled: 11/15/01 <br /> 837 Shaw Road Date Received: 11/16/01 <br /> Stockton, CA 95215 Client Contact Suzanne Henderson Date Extracted: 11/16/01 <br /> Client P.O: Date Analyzed: 11/19-11/21/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 83734 <br /> Client ID HAI-6 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* Rgord,U` <br /> W 5 W S <br /> Acetone ND<100 5.0 1 25 trans-1,3-Dichlompropene ND<20 1.0 5.0 <br /> Benzene ND<0 1.0 5.0 Ethylene dibrontide ND<20 1.0 5.0 <br /> 13mmobenzeoe ND<20 1.0 5.0 Ethylbenzene ND<20 1.0 5.0 <br /> Bromochlommethane ND<20 1.0 5.0 Hexachlombutadiene ND<100 5.0 25 <br /> Brornodichloromethane ND<20 1.0 5.0 lodomethane ND<20 1.0 - 5.0 <br /> Bromoform ND<20 1.0 5.0 Isopropyibenzene ND<20 1.0 5.0 <br /> Bromomethane ND<20 1.0 5.0 p-Isopropyl toluene ND<20 1.0 5.0 <br /> n-Butyl benzene ND<20 1.0 5.0 Methyl butyl ketone IQ ND<20 LO 5.0 <br /> sec-Butyl benzene 150 1.0 5.0 Methylene Chloride` ND<20 1.0 5.0 <br /> tert-Butyl benzene ND<20 1.0 5.0 Methyl ethyl ketone ND<40 2.0 l0 <br /> Carbon Disulfide ND<20 1.0 5.0 Methyl isobutyl ketones ND<20 1.0 5.0 <br /> Carbon Tetrachloride ND<20 Lo 5.0 Methyl tert-Butyl Ether(MTBE) - 1.0 5.0 <br /> Chlombenzene ND<20 1.0 5.0 Naphthalene ND<100 5.0 25 <br /> Chloroethane ND<20 LO 5.0 n-Propyl berzme 71 1.0 5.0 <br /> 2-Chlomethyl Vinyl Etherr` ND<20 10 --5 0 Styrene ND<20 1.0 5.0 <br /> ChloroformND<20 LO 5.0 1,1,1,2-Tetrachloroethane ND<20 1.0 5.0 <br /> Chloromethane ND<0 1.0 5.0 1,1,2,2-Tetrachloroethane ND<20 1.0 5.0 <br /> 2-Chlomtolume ND<20 1.0 5.0 Tetrachloroethme 95<20 1.0 S.D <br /> 4-Chlormoluene ND<20 1.0 5.0 Toluene ND<20 1.0 5.0 <br /> Dibromochlommethme ND<20 1.0 5.0 1,2,3-Tnchlombenzene ND<100 5.0 25 <br /> 1,2-Dibromo-3-chlompropane ND<40 2.0 10 1,2,4-Trichlomberzene ND<100 5.0 25 <br /> Dibromomethane ND<20 1.0 5.0 1,1,1-Trichloroethane ND<20 1.0 5.0 <br /> 1,2-Dichlombenzme ND<20 1.0 5.0 1,1,2-Trichloroethane ND<20 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<20 1.0 5.0 Trichloroethene ND<20 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<0 1.0 5.0 Trichlorofluoromethane ND<20 1.0 5.0 <br /> Dichlorodifluoromethane ND<0 1 1.0 5.0 1,2,3-Trichloropropzne ND<20 1.0 -370- <br /> 1,1-Dichlomethm <br /> .01,1-Dichlomethme RND<201.0 5.0 1,2,4-Trimethylbmzene 410 1.0 5.0 <br /> l,2-Dichloroethane1.0 5.0 1,35-Trimethylbenzene ND<20 1.0 5.0 <br /> 1,1-Dichlomethene1.0 5.0 Vinyl Acetate '° NiX100 5.0 25 <br /> cis-l,2-Dichloroethene 1.0 5.0 Vinyl Chloride " ND<20 10 5.0 <br /> [cans-l,2-Dichlomethene 1.0 5.0 Xylenes,total �° ND<20 1.0 5.0 <br /> 1,2-Dichloropropane 1.0 5.0 Comments: <br /> 1,3-Dichlomp upane LO 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichlompropane 1.0 5.0 Dibmmofluoromethane 113 <br /> l,l-Dichloropropene 1.0 5.0 Toluene-d8 98 <br /> cis-1,3-Dicb1oropropene N0<0 1.0 5.0 4-Bromofluorobenzene 75 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chlomethoxy) ethme; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pmtanone or isopropylacetone; (h)lighter than water immiscable sheen is present; (i) liquid sample that contains greater than-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 0) methylbenzene; (m) acetic acid ethinyl ester, (n) <br /> chloroethme;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />