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MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> 1 0 0 005�6;1 <br /> I vast W s <br /> r r nv�!ci. ,r Qq m I D o m5' .y s o b Z S-3 � �s b I,-z.� p,n � •% <br /> T K TANK TPH-G TPH-D BTX 3c E CL HC TOTAL EDB METAS PCB <br /> # CONTENTS 8015 8015 8020 8010 LEAD ICAP/ 8270 <br /> 8260 8260 8260 8240 7420 8240 AES or 8080 <br /> 7421 AA <br /> LEADED <br /> GAS X X X :C <br /> UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X <br /> J v ,Uls OIL X X <br /> CHLOR <br /> SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X <br /> 40 <br /> S,�lla� WASTES _ <br /> USED OIL x X X X Y X <br /> ,41Aou k 4G rl orG r�+ f s 1- was a iL !'� was pv�•�c <br /> alyses methods are designated EPA metiods described in EPA SW 846, Third Edition Those methods not found in <br /> SW 846, are specifically noted below Refer to the "SWRCB LUFT Field Manual", Appendix A-20, Table 3-5 for detection <br /> t <br /> mits of motor vehicle fuels (gasoline and diesel) Refer to 1-2-3 "Regional Board Staff Recommendations for Initial <br /> valuation and Investigation of US7s" for the waste and motor oil detection limits <br /> Detection Limits that remain below the MCL, STLC or Allowable Lima of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method <br /> LABORATORY ANALYSES TERMINOLOGY <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 3015 mod or GCII�IS 8260 <br /> VH-D Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GCIMS 8260 <br />!gam & E Benzene, Toluene, Xyiene & Ethyl Benzene, GC/PID 8020 or GCIMS 3260 <br /> CL HC Chlorinated Hydrocarbon, GCIHSD 8010, GC/MS 5240 <br /> VOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide (DHS-AB 1803), GCIMS 8240 (DHS-Luft) <br /> rPCB <br /> Gas Chromatography, Flame Ionization Detection <br /> Inductively Coupled Plasm Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000 etal Cadmium Chromium III -snd VI Lead Zinc and Ntckei. <br /> Polychlorinated Btphenyls, C/MS 8270 or 8080 <br /> Itylethad 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> IQA/QC Quality Assurance/Quality Control <br /> pes To avoid false positive detection of benzene, benzene-free solvents are to be used Fused capillary columns are <br /> erred to packed columns, a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> e been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 series <br /> because the detection limits are lower the QA/QC is better <br /> I�EH 23 048 (Rev 218191) Page 8 <br />