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Y <br /> / MINIMUM VERIFICATION LABORATORY ANALYSI! Vgaib <br /> Ds <br /> r L C rBC7W ( La wax- I.rr it �D,a.,t o g:sr p" s O b 2 5-s * 1S b _Z <br /> T K TANK TPH-G TPH-D BTX & E CL HC TO'T'AL EDF { IvIEI'Ai 5 PCs <br /> # CONTENTS 8015 8015 8020 8014 LEADICAFf 8270 <br /> 3260 8260 8260 8240 7420 8z40 AES or 8080 <br /> 7421 AA <br /> I , 6 LEADED <br /> GAS X X X X <br /> UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X <br /> .4'VAree OIL X X <br /> CHLOR. <br /> SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X <br /> it <br /> S, !!v, WASTEI <br /> .10 USED OIL X X X X X <br /> ,4;Apu.l4 #i& 14 7M om,.r,4 .Os t2 d� As-44 ou- 117 WA.s K- 7V � <br /> AjWalyses methods are designated EPA melods described in EPA SW W,TbI Edition. Those methods not found in <br /> SW 846, are specifically noted below. Refer to the "SWRCB LUFT Field Manual",Appendix A-20, Table 3-5 for dcucilon <br /> limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 'Regional Board Staff Recommendations for Initial <br /> Evaluation and Investigation of UST`s" for the waste and motor at] detection limits <br /> Detection limits that remain below the MCI., STLC or Allowable Limit of the contaminant in g3estiort will be acceptea, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TER VIINOLOGY. <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline, GCIFID (5030) 8015 mod or GCIMS 3260 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GCJMS 8260 <br /> BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, GCIPM 3020 or GC/MS 3260 <br /> CL HC Chlonnated Hydrocarbon, GClHSD 8010, GCJMS 3240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide (DHS-AB 1803), GC/MS 8240 (DHS-Luft) <br /> G - Gas Chromatography, Flame Ionization Detestton <br /> CAP or Inductively Coupled Plan Atomic Emission Spectrometry 6010 or Atonuc Absorption <br /> Spectrometry 7000. etas Cadmium-Chromium m 111 2nd YL Lead, Zinc and Nickel. <br /> PCB Poiychlontiated 13ipheny CIMS 8270 or 8080 - <br /> Method 3050 Aad digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QAJQC Quality Assurance/Quality Control <br /> To avoid false positive detection of benzene, benzene-free solvents are to be used Fused capillary columns are <br /> rred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QAIAC is followed <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 series <br /> because the detection limits are lower the QA/QC is better. <br /> EH 23 048 (Rev 218191) Page 9 <br />