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1 A13 POSITIVE 781 East Washington Blvd , Los Angeles, CA 90021 LAB SERVICE (213) 745-5312 FAX (213) 745-6372 I ' CERTIFICATE OF ANALYSIS Orion Environmental, Inc. 01/16/01 ' File# 73287 3450 East Spring Street, Suite 212 No. 11ST PO#SA Long Beach CA 90806 BFS-Stockton Attn: Harry Takach Phone: (562) 988-2755 Fax: (562)988-2759 1,3-Dichlorobenzene EPA 50308 EPA 82608 NO ug/1 1 ' 4-Isopropyl toluene EPA 5030B EPA 82606 NO ug/1 1 1,4-Dichlorobenzene EPA 5030B EPA 82606 ND ug/l 1 I 1,2-Dichlorobenzene EPA 5030B EPA 82608 NO ug/l 1 n-Butylbenzene EPA 5030B EPA 82606 NO ug/1 1 1,2-D1bromo-3-chloroprop8ne EPA 50306 EPA 82606 NO ug/l 1 1,2,4-Tnchlorobenzene EPA 5030B EPA 82608 NO ug/l 1 Hexachlorobutadiene EPA 50306 EPA 82606 NO ug/l 1 Naphthalene EPA 50308 EPA 82608 ND ug/l 1 1,2,3-Tnchlorobenzene EPA 50306 EPA 82608 NO ug/l 1 MTBE EPA 50306 EPA 82608 NO ug/1 1 1,4-Dioxane EPA 50306 EPA 82608 NO ug/1 10 Surrogates EPA 5030B EPA 8260B Dibromofluoromethane EPA 5030B EPA 8260B 112 Percent Toluene D-8 EPA 5030B EPA 8260B 100 Percent 4-Bromofluorobenzene EPA 50306 EPA 8260B 106 Percent Sample* 20010076-004 Collector w Method Received 01/09/2001 Sampling Date/Time Type. Water I D Method Blank ,Par4Meter , .... »„ Prgp1TeA M;gthod , Result. Unit PQk, Prep Date: 01/16/2001 Analysis Date- 01/16/2001 TPH-Gasoline EPA 50306 EPA 80158 ND ug/l SO Surrogates EPA 50306 EPA 80158 Tnfluorotoluene EPA 50306 EPA 80156 125 Percent Prep Date: 01/16/2001 Analysis Date: 01/16/2001 Dichlorodifluoromethane EPA 50308 EPA 82606 NO ug/l 1 Chloromethane EPA 50306 EPA 82608 NO ug/l 1 Vinyl chloride EPA 5030B EPA 8260B NO ug/1 0 5 Bromomethane EPA 5030B EPA 82606 NO ug/l 1 Chloroethane EPA 5030B EPA 82606 NO ug/1 1 Tnchlorofluoromethane EPA 5030B EPA 82606 NO ug/l 1 Acetone EPA 50306 EPA 82608 NO ug/l 10 8 20010076-004