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POSITIVE 781 East Washington Blvd , Los Angeles, CA 90021 LAB SERVICE (213) 745-5312 FAX (213) 745-6372 CERTIFICATE OF ANALYSIS Orion Environmental, Inc. 09/14/00 File* 73287 3450 East Spring Street, Suite 212 Pry, No. 115T ' Long Beach CA 90806 BFS-Stockton Attn: Harry Takach Phone: (562) 988-2755 Fax: (562) 988-2759 Sample*: 20001898-001 Collector Client Method Picked Up By PLS Received: 09/07/2000 Sampling Date/Time 09/06/2000 1 05 00 PM Type Water 10 MW-2 Parameter Prep/Test Method Re51,11t I)nit PQ4 Prep Date: 09/12/2000 Analysis Date: 09/12/2000 TPH-Gasoline EPA 5030B EPA 8015B 430 ug/I 50 ' Surrogates EPA 5030B EPA 8015B Tnfluorotoluene EPA 50308 EPA 80156 115 Percent Prep Date: 09/12/2000 Analysis Date: 09/12/2000 Dichlorodifluoromethane EPA 5030B EPA 8260B NO ug/I 1 Chloromethane EPA 50306 EPA 8260B NO ug/l 1 Vinyl chlonde EPA 5030B EPA 82606 NO ug/I 05 Bromomethane EPA 5030B EPA 82608 NO ug/I 1 Chloroethane EPA 5030B EPA 82608 NO ug/I 1 Trichlorofluoromethane EPA 50306 EPA 8260B NO ug/1 1 Acetone EPA 50308 EPA 8260B NO ug/1 10 Carbon disulfide EPA 50308 EPA 82605 NO ug/1 5 1,1-Dichloroethene EPA 50308 EPA 82606 NO ug/I 1 Methylene chloride EPA 5030B EPA 82606 74 ug/I 25 trans-l,2-dichloroethene EPA 5030B EPA 82606 NO ug/l 1 ' 1,1-Dichloroethane EPA 5030B EPA 82608 NO ug/I 1 Vinyl acetate EPA 5030B EPA 82608 ND ug/I 5 2,2-Dichloropropane EPA 50306 EPA 8260B NO ug/1 1 cis-1,2-Dichloroethene EPA 50306 EPA 8260B NO ug/I 1 2-Butanone EPA 50308 EPA 8260B NO ug/I 5 ' Bromochloromethane EPA 50308 EPA 8260B NO ug/1 1 Chloroform EPA 5030B EPA 82606 12 ug/I 1 1,1,1-Tnchloroethane EPA 50306 EPA 8260B NO ug/I 1 Carbon tetrachloride EPA 5030B EPA 8260B NO ug/1 0 5 1,1-Dichloropropene EPA 5030B EPA 8260B ND ug/1 1 Benzene EPA 5030B EPA 8260B NO ug/I 1 1,2-Dichloroethane EPA 5030B EPA 8260B ND ug/I 0 5 1 20001898-001