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� 0 POSITIVE ' 781 East Washington Blvd , Los Angeles, CA 90021 LAB SERVICE (213) 745-5312 FAX (21 3) 745-6372 CERTIFICATE OF ANALYSIS ' Orion Environmental, Inc. 09/14/00 File# 73287 ' 3450 East Spring Street, Suite 212 Prj. No. 11ST Long Beach CA 90806 BFS-Stockton ' Attn: Harry Takach Phone: (562) 988-2755 Fax: (562) 988-2759 1,4-Dioxane EPA 50306 EPA 8260B ND ug/I 10 ' tert-Butyl alcohol EPA 50306 EPA 82603 ND ug/I 5 Di-isopropyl ether EPA 5030B EPA 8260B ND ug/I 1 ' tert- Butyl ethyl ether EPA 5030B EPA 82606 ND ug/1 1 tert-Amyl methyl ether EPA 50306 EPA 8260B ND ug/1 1 Surrogates EPA 50308 EPA 8260B Dibromofluoromethane EPA 50308 EPA 62606 113 Percent Toluene D-8 EPA 5030B EPA 82606 100 Percent 4-Sromofluorobenzene EPA 5030B EPA 8260B 102 Percent 10 Prep Date: Analysis Date- Ethylene Dibromide � EPA 3510 EPA 504 1mwmSee Attachment 002 Sample* 20001898-003 Collector Client Method Picked Up By PLS Received 09/07/2000 Sampling Date/Time 09/06/2000 2 40 00 PM Type Water I D MW-1 Parameter Prep]Test Method Result Unit PQ4 Prep Date: 09/12/2000 Analysis Date 09/12/2000 ' TPH-Gasoline EPA 5030B EPA 80156 ND ug/I 50 Surrogates EPA 5030B EPA 8015B ' Tnfluorotoluene EPA 50306 EPA 80156 107 Percent Prep Date: 09/12/2000 Analysis Date- 09/12/2000 Dichlorodifluoromethane EPA 50306 EPA 8260B ND ug/I 1 Chloromethane EPA 50306 EPA 8260B ND ug/1 1 Vinyl chloride EPA 50306 EPA 82606 ND ug/I 05 ' Bromomethane EPA 50306 EPA 8260B ND ug/I 1 Chloroethane EPA 50308 EPA 8260B ND ug/I 1 Tnchlorofluoromethane EPA 5030B EPA 82606 ND ug/I 1 ' Acetone EPA 5030E EPA 82608 ND ug/l 10 Carbon disulfide EPA 5030B EPA 82608 ND ug/l 5 . 1,1-Dichloroethene EPA 50308 EPA 82608 ND ug/I 1 Methylene chloride EPA 50306 EPA 82606 22 ug/I 25 trans-l,2-dichloroethene EPA 50306 EPA 8260B ND ug/I 1 1,1-Dichloroethane EPA 50300 EPA 82606 ND ug/I 1 ' 6 20001898-003