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110 2nd Avenue South #D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> http/jwwwmccampbe1lcom ]`mail mam®mccampbell cam <br /> _Ljt <br /> QC SUMMARY REPORT FOR SW8260B <br /> Matrix W WorkOrder 0303023 <br />' EPA Method SW8260B Extraction SW5030B BatchlD 6057 Spiked Sample ID N/A <br /> Sample Spiked MS` MSD' MS-MSD' LCS LCSD LCS-LCSD Acceptance Criteria(°�) <br /> Compound <br /> "glL uglL %Rec 9/6 Rec -/.RPD %Rec %Rec %RPD tow High <br /> Benzene NIA 10 N/A NIA NIA 106 106 000301 70 130 <br /> tcrt-Amyl methyl ether(TAME) NIA 10 NIA NIA NIA 793 766 349 70 — 130 <br /> Methyl-t-butyl ether(MTBE) N/A 10 NIA NIA NIA 772 75 7 199 70 130 <br /> Toluene NIA 10 N/A NIA NIA 955 95 5 00236 70 130 <br /> Dusopropyl ether(DIPE) N/A 10 N/A NIA NIA 961 964 0 386 70 130 <br /> Ethyl tert-butyl ether(ETBE) NIA !0 N/A NIA NIA 858 84 6 151 70 130 <br /> %SSI N/A 100 N/A N/A N/A 989 97 5 144 70 130 <br /> %SS2 NIA 100 NIA N/A N/A 107 108 0 676 70 130 <br />' %SS3 NIA 100 NIA NIA NIA 965 962 0 346 70 130 <br /> • All target compounds m the Method Blank of this extraction batch were NI)less than the method RL with the following exceptions <br /> NONE <br /> MS=Matrix Spike,MSD=Matrix Spike Duplicate LCS.=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=7PercentDeviabon <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicateNR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted du <br /> ' analyte content <br /> %Recovery=10o'(MS-Sample)I(Amount Spiked) RPD=100'(MS–MSD)I(M$+MSD).2 <br /> 'MS and I or MSD spike recovenes may not be near 100%or the RPDs near 0%it-a)the sample is inhomogenous AND contains significant concentrations of <br /> ' analyte relative to the amount spiked or b)if that specific sample matrix interferes with spike recovery <br />